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芳香新塔花药材质量标准的研究
引用本文:杨伟俊,何江,满尔哈巴,阿不都沙拉木,毛燕,于睿.芳香新塔花药材质量标准的研究[J].中国实验方剂学杂志,2010,16(10):65-68.
作者姓名:杨伟俊  何江  满尔哈巴  阿不都沙拉木  毛燕  于睿
作者单位:1. 新疆维吾尔自治区药物研究所,乌鲁木齐,830004;新疆维吾尔药重点实验室,乌鲁木齐,830004
2. 新疆维吾尔自治区药物研究所,乌鲁木齐,830004
基金项目:新疆维吾尔自治区科技基础条件平台建设项目,新疆维吾尔药实验室课题 
摘    要:目的:制定芳香新塔花药材的质量标准,为该药用植物的资源开发和合理利用提供科学依据。方法:生药学研究,水分测定,灰分测定,薄层色谱法,高效液相色谱法测定。结果:对芳香新塔花的性状、显微特征、薄层特征进行了描述;对总灰分、酸不溶性灰分和水分进行了测定;高效液相色谱法测定金合欢素含量的线性范围为1.168~12.848mg·L-1,加样回收率为100.87%,RSD为2.19%;结论:本质量控制方法可以用来评价芳香新塔花药材的质量。

关 键 词:芳香新塔花  质量标准  显微鉴别  薄层色谱  金合欢素  高效液相色谱法
收稿时间:2009/12/27 0:00:00

Study on Quality Specification of Ziziphora clinopodioides Lam.
YANG Wei-jun,HE Jiang,Manerhab,Abudushalamu,MAO Yan and YU Rui.Study on Quality Specification of Ziziphora clinopodioides Lam.[J].China Journal of Experimental Traditional Medical Formulae,2010,16(10):65-68.
Authors:YANG Wei-jun  HE Jiang  Manerhab  Abudushalamu  MAO Yan and YU Rui
Abstract:Objective: To provide scientific basis for the utilization and development of Ziziphora clinopodioides by setting up the quality control specification of Z. clinopodioides. Method: The pharmacognostical methods were applied,moisture and ash were determined. And the constituents were analyzed by TLC and HPLC. Result: The morphological,histological and TLC characters of Z. clinopodioides. were observed. Content of total ash,acid-insoluble ash,and moisture were determined. The content of acacetin was determined by HPLC,with good linearity between 1.168-12.848 mg·L-1. The average recovery of chrysophanol was 100.87%, and RSD was 2.19%,respectively. Concusion: The method developed can be used for the quality control of Z. clinopodioides.
Keywords:Ziziphora clinopodioides  quality specification  microscopical identifcation  TLC  acacetin  HPLC
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