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妇炎清洗剂的质量标准研究
引用本文:汪加龙,刘丛彬. 妇炎清洗剂的质量标准研究[J]. 安徽医药, 2011, 15(9): 1173-1175
作者姓名:汪加龙  刘丛彬
作者单位:汪加龙,WANG Jia-long(安徽省舒城县人民医院药剂科,安徽,舒城,231300);刘丛彬,LIU Cong-bin(安徽中医学院药学院,安徽,合肥,230038)
摘    要:目的建立妇炎清洗剂的质量标准。方法采用薄层色谱法(TLC)对妇炎清洗剂中苦参、黄柏、白鲜皮、龙胆进行鉴别;用HPLC法对妇炎清洗剂中蛇床子的成分蛇床子素含量进行测定。结果薄层色谱中斑点清晰,易于观察。蛇床子素的进样浓度在5.92~59.20 mg·L-1范围内,与峰面积呈良好的线性关系(r=0.999 6);平均回收率为98.83%,RSD=0.65%(n=6)。结论该方法简单可行、重复性好,能有效地控制妇炎清洗剂的质量。

关 键 词:妇炎清洗剂  薄层色谱法  高效液相色谱法  质量标准

Quality standard for Fuyanqing lotion
WANG Jia-long,LIU Cong-bin. Quality standard for Fuyanqing lotion[J]. Anhui Medical and Pharmaceutical Journal, 2011, 15(9): 1173-1175
Authors:WANG Jia-long  LIU Cong-bin
Affiliation:1.Pharmacy Department,People's Hospital of Shucheng,Shucheng,Anhui 231300,China; 2.School of Pharmacy,Anhui College of Traditional Chinese Medicine,Hefei,Anhui 230038,China)
Abstract:Aim To establish the quality standard for Fuyanqing lotion.Methods The sophora,Phellodendron amurense,Cortex Dictamni and gentian in Fuyanqing lotion were identified by TLC,and content of Osthol of selinum japenious seed in Fuyanqing lotion was determined by HPLC.Results The spots in the TLC were clear and distinguished well.The linear range of Osthol was 5.92~59.20 mg·L-1(r=0.999 6).The average recovery was 98.83%,and RSD was 0.65%(n=6).Conclusion The method is simple and repeatable,which can be used for the quality control of Fuyanqing lotion.
Keywords:Fuyanqing lotion  TLC  HPLC  the quality standard
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