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| 醋狼毒饮片质量标准研究 | |
| 引用本文： | 邓英君,庄果,汪兰云,李俊松,蔡宝昌,葛乃贵. 醋狼毒饮片质量标准研究[J]. 中国实验方剂学杂志, 2012, 18(23): 98-101 |
| 作者姓名： | 邓英君 庄果 汪兰云 李俊松 蔡宝昌 葛乃贵 |
| 作者单位： | 1. 南京市中医院,南京,210001 2. 南京中医药大学江苏省中药炮制重点实验室,南京,210029 3. 江苏省海安针灸推拿学校,江苏南通,226600 |
| 基金项目： | 国家公益性行业专项基金项目(200807039);南京中医药大学中药学一级学科开放课题(2011ZYX2-011) |
| 摘 要： | 目的:制订醋狼毒饮片的质量标准。方法:收集炮制10批醋狼毒饮片,对水分、总灰分、酸不溶性灰分、浸出物进行测定,并以狼毒乙素含量为指标进行含量测定。结果:拟定醋狼毒饮片水分不得超过9.12%,总灰分不得超过6.50%,酸不溶性灰分不得超过1.09%,醇溶性浸出物不少于7.70%,狼毒乙素含量不少于0.038%。结论:初步建立醋狼毒饮片量化质控标准评价体系。 |
| 关 键 词： | 醋狼毒 质量标准 含量测定 |
| 收稿时间： | 2012-06-26 |
Study on Quality Standard of Vinegar Backed Euphorbia Ebracteolata |
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| DENG Ying-jun,ZHUANG Guo,WANG Lan-yun,LI Jun-song,CAI Bao-chang and GE Nai-gui. Study on Quality Standard of Vinegar Backed Euphorbia Ebracteolata[J]. China Journal of Experimental Traditional Medical Formulae, 2012, 18(23): 98-101 | |
| Authors: | DENG Ying-jun ZHUANG Guo WANG Lan-yun LI Jun-song CAI Bao-chang GE Nai-gui |
| Affiliation: | 1.Nanjing Hospital of Traditional Chinese Medicine,Nanjing 210001,China; 2.Nanjing University of Traditional Chinese Medicine,Jiangsu Key Laboratory of Chinese Medicine Processing, National First-Class Key Discipline for Traditional Chinese Medicine of Nanjing University of Chinese Medicine,Nanjing 210029,China; 3.Jiangsu Province Hai’an Acupuncture Massage School,Nantong 226600,China) |
| Abstract: | Objective: To revise and improve the quality standard of vinegar backed E. ebracteolata. Method: 10 batches of vinegar backed Euphorbia ebracteolata were investigated with TLC. Moisture content, total ash, acid-insoluble ash and extractum were explored. The content of ebracteolata cpd B was determined by HPLC. Result: The quality standard was preliminarily formulated as follows: the moisture content should not pass 9.12%. Total ash should not pass 6.50%. Acid-insoluble ash should not pass 1.09%. Alcohol-soluble extractive should not lower than 7.70%. The content of ebracteolata cpd B should not lower than 0.038%. Conclusion: Quality control quantization evaluation system of processed E. ebracteolata slice is preliminarily established. |
| Keywords: | vinegar backed Euphorbia ebracteolata quality standards content |
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