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醋狼毒饮片质量标准研究
引用本文:邓英君,庄果,汪兰云,李俊松,蔡宝昌,葛乃贵.醋狼毒饮片质量标准研究[J].中国实验方剂学杂志,2012,18(23):98-101.
作者姓名:邓英君  庄果  汪兰云  李俊松  蔡宝昌  葛乃贵
作者单位:1. 南京市中医院,南京,210001
2. 南京中医药大学江苏省中药炮制重点实验室,南京,210029
3. 江苏省海安针灸推拿学校,江苏南通,226600
基金项目:国家公益性行业专项基金项目(200807039);南京中医药大学中药学一级学科开放课题(2011ZYX2-011)
摘    要:目的:制订醋狼毒饮片的质量标准。方法:收集炮制10批醋狼毒饮片,对水分、总灰分、酸不溶性灰分、浸出物进行测定,并以狼毒乙素含量为指标进行含量测定。结果:拟定醋狼毒饮片水分不得超过9.12%,总灰分不得超过6.50%,酸不溶性灰分不得超过1.09%,醇溶性浸出物不少于7.70%,狼毒乙素含量不少于0.038%。结论:初步建立醋狼毒饮片量化质控标准评价体系。

关 键 词:醋狼毒  质量标准  含量测定
收稿时间:2012/6/26 0:00:00

Study on Quality Standard of Vinegar Backed Euphorbia Ebracteolata
DENG Ying-jun,ZHUANG Guo,WANG Lan-yun,LI Jun-song,CAI Bao-chang and GE Nai-gui.Study on Quality Standard of Vinegar Backed Euphorbia Ebracteolata[J].China Journal of Experimental Traditional Medical Formulae,2012,18(23):98-101.
Authors:DENG Ying-jun  ZHUANG Guo  WANG Lan-yun  LI Jun-song  CAI Bao-chang and GE Nai-gui
Institution:1.Nanjing Hospital of Traditional Chinese Medicine,Nanjing 210001,China; 2.Nanjing University of Traditional Chinese Medicine,Jiangsu Key Laboratory of Chinese Medicine Processing, National First-Class Key Discipline for Traditional Chinese Medicine of Nanjing University of Chinese Medicine,Nanjing 210029,China; 3.Jiangsu Province Hai’an Acupuncture Massage School,Nantong 226600,China)
Abstract:Objective: To revise and improve the quality standard of vinegar backed E. ebracteolata. Method: 10 batches of vinegar backed Euphorbia ebracteolata were investigated with TLC. Moisture content, total ash, acid-insoluble ash and extractum were explored. The content of ebracteolata cpd B was determined by HPLC. Result: The quality standard was preliminarily formulated as follows: the moisture content should not pass 9.12%. Total ash should not pass 6.50%. Acid-insoluble ash should not pass 1.09%. Alcohol-soluble extractive should not lower than 7.70%. The content of ebracteolata cpd B should not lower than 0.038%. Conclusion: Quality control quantization evaluation system of processed E. ebracteolata slice is preliminarily established.
Keywords:vinegar backed Euphorbia ebracteolata  quality standards  content
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