| 痛风颗粒质量标准研究 |
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| 引用本文： | 张义生,张荒生,王进军.痛风颗粒质量标准研究[J].中国药房,2009(6):448-449. |
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| 作者姓名： | 张义生 张荒生 王进军 |
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| 作者单位： | 武汉市中医医院,武汉市430014 |
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| 摘 要： | 目的:建立痛风颗粒的质量标准。方法:采用薄层色谱(TLC)法对方中薏苡仁、赤芍、甘草进行定性鉴别;采用高效液相色谱-蒸发光散射检测法测定知母中有效成分菝葜皂苷元的含量。结果:TLC特征明显、专属性强;菝葜皂苷元进样量在0.546～4.368μg范围内与峰面积积分值呈良好的线性关系(r=0.9998);平均回收率为97.74%,RSD=1.3%(n=6)。结论:所建标准可用于痛风颗粒的质量控制。
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| 关 键 词： | 痛风颗粒 薄层色谱法 高效液相色谱法 质量标准 |
Quality Standard of Tongfeng Granules |
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| ZHANG Yi-sheng,ZHANG Huang-sheng,WANG Jin-jun.Quality Standard of Tongfeng Granules[J].China Pharmacy,2009(6):448-449. |
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| Authors: | ZHANG Yi-sheng ZHANG Huang-sheng WANG Jin-jun |
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| Institution: | (Wuhan Hospital of Traditional Chinese Medicine, Wuhan 430014, China) |
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| Abstract: | OBJECTIVE：To establish the quality standard of Tongfeng granules.METHODS：Coix lacryma - jobi ,Radix Paeoniae Rubra and Radix et Rhizoma Glycyrrhizae in the granules were identified by TLC, and the content of sarsasapogenin in Tongfeng granules was determined by HPLC- ELSD .RESULTS：The TLC characteristics were distinctive and specific .The linear range for sarsasapogenin was 0.546-4.368 μg（ r = 0.999 8） and the average recovery was 97.74% （RSD = 1.3%, n = 6）.CONCLUSION： The established standard can be used for the quality control of Tongfeng granules. |
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| Keywords: | Tongfeng granules TLC HPLC Quality standard |
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