| 七味抗体散质量标准研究 |
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| 引用本文： | 范荣,薛晓会.七味抗体散质量标准研究[J].中国药房,2009(3):215-216. |
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| 作者姓名： | 范荣 薛晓会 |
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| 作者单位： | 河南平顶山市食品药品检验所,平顶山市467000 |
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| 摘 要： | 目的:建立七味抗体散的质量标准。方法:采用薄层色谱(TLC)法对方中黄芪、当归、丹参3味药材进行定性鉴别;用高效液相色谱法对方中丹参的主要成分丹参酮ⅡA进行含量测定。结果:TLC特征斑点明显。丹参酮ⅡA的检测浓度在5.44～32.64μg.mL-1范围内与峰面积积分值呈良好的线性关系(r=0.9998);平均回收率为99.54%,RSD=0.96%(n=9)。结论:所建质量标准可用于七味抗体散的质量控制。
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| 关 键 词： | 七味抗体散 质量标准 薄层色谱法 高效液相色谱法 |
Quality Standard of Qiwei Kangti Powders |
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| FAN Rong,XUE Xiao-hui.Quality Standard of Qiwei Kangti Powders[J].China Pharmacy,2009(3):215-216. |
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| Authors: | FAN Rong XUE Xiao-hui |
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| Institution: | (Henan Pingdingshan Institute for Food and Drug Control,Pingdingshan 467000, China) |
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| Abstract: | OBJECTIVE： To establish the quality standard for Qiwei kangti powders.METHODS： Radix Astragali, Angelica sinensis, Salvia miltiorrhiza were identified by TLC.The content of tanshinone ⅡA（the chief content in Salvia miltiorrhiza ） was determined by HPLC.RESULTS： The TLC spots developed were fairly specific. Tanshinone ⅡA showed a good linear relationship at a range of 5.44～32.64μg·mL^-1（ r = 0.999 8）, and its average recovery was 99.54% （RSD = 0.955%, n = 9）.CONCLUSION：The established quality standard is applicable for the quality control of Qiwei kangti powders. |
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| Keywords: | Qiwei kangti powders Quality standard TLC HPLC |
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