| 脑清通胶囊质量标准研究 |
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| 引用本文： | 王婴,王岩.脑清通胶囊质量标准研究[J].广东药学院学报,2011,27(3):288-291. |
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| 作者姓名： | 王婴 王岩 |
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| 作者单位： | 1. 广东药学院医药化工学院,广东广州,510006
2. 广东药学院中药学院,广东广州,510006 |
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| 基金项目： | 广东药学院人才引进启动基金，广东药学院师资队伍建设经费资助 |
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| 摘 要： | 目的 建立脑清通胶囊的质量标准.方法 采用薄层色谱法鉴别脑清通胶囊中的石菖蒲、山茱萸、枳实、甘草;采用高效液相色谱法测定脑清通胶囊中丹酚酸B的含量.结果 在薄层色谱中检出了石菖蒲、山茱萸、枳实、甘草的特征斑点;高效液相色谱法测出丹酚酸B在0.448-5.6μg范围内与峰面积线性关系良好,r=0.999 9,平均回收率为...
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| 关 键 词： | 脑清通胶囊 薄层色谱法 高效液相色谱法 质量标准 |
Study on the quality standard of Naoqingtong capsule |
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| WANG Ying,WANG Yan.Study on the quality standard of Naoqingtong capsule[J].Academic Journal of Guangdong College of Pharmacy,2011,27(3):288-291. |
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| Authors: | WANG Ying WANG Yan |
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| Institution: | 1.School of Pharmaceutical and Chemical Engineering,Guangdong Pharmaceutical University,Guangzhou 510006,China;2.School of Traditional Chinese Medicine,Guangdong Pharmaceutical University,Guangzhou 510006,China) |
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| Abstract: | Objective To establish the quality standard of Naoqingtong capsule.Methods Thin layer chromatography（TLC） was performed to identify Rhizoma acori tatarinowii,Fructus corni,Fructus aurantii immaturus and Radix glycyrrhizae in Naoqingtong capsule.Salvianolic acid B was determined by high performance liquid chromatography（HPLC）.Results Rhizoma acori tatarinowii,Fructus corni,Fructus aurantii immaturus and Radix glycyrrhizae can be detected by TLC;The calibration curve of HPLC was linear in the range of 0.448-5.6 μg（r = 0.999 9）.The average recovery rate and RSD was 96.9% and 1.17%.Conclusion The method is simple,accurate and specific.It can be used for the quality control of Naoqingtong capsule effectively. |
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| Keywords: | Naoqingtong capsule TLC HPLC quality standard |
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