| 抗病毒合剂质量标准研究 |
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| 引用本文： | 李全斌,易生富,李纪元,杨远荣,孙亚楠.抗病毒合剂质量标准研究[J].辽宁中医学院学报,2013(7):76-78. |
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| 作者姓名： | 李全斌 易生富 李纪元 杨远荣 孙亚楠 |
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| 作者单位： | [1]湖北中医药高等专科学校,湖北荆州434020 [2]华中科技大学同济医学院附属荆州医院,湖北荆州434020 |
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| 摘 要： | 目的：建立抗病毒合剂的质量标准。方法：采用TLC法对处方中的板蓝根、黄芪进行鉴别,用分光光度法测定制剂中的黄芪甲苷。结果：TLC法斑点清晰、专属性强、阴性对照无干扰;黄芪甲苷的含量在4.182~41.82μg.mL-1范围内线性关系良好（r=0.9992）,平均回收率为99.7%,RSD=0.96%（n=5）。结论：该法简单、结果准确、重现性好、可用于抗病毒合剂的质量控制。
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| 关 键 词： | 抗病毒合剂 薄层色谱 板蓝根 黄芪 黄芪甲苷 |
Quality Standard Study on Kangbingdu Mixture |
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| Institution: | LI Quanbin, YI Shengfu, LI Jiyuan, YANG Yuanrong, SUN Ya＇nan ( 1.Hubei College of Traditional Chinese Medicine, Jingzhou 434020, Hubei, China; 2.Jingzhou Hospital, Tongji Medical College, Huazhong University of Science and Technology, Jingzhou 434020, Hubei, China ) |
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| Abstract: | Objective： To establish a quality standard for Kangbingdu Mixture. Methods：The Radix astragali and Radix isatidis were identified by TLC and Astragaloside IV was determined by spectrometric method. Results：Thin layer chromatography spots were clear, with high specificity, while the negative control showed no interferenee.Astragaloside IV showed a good linear relationship within the range of 4.182 to 41.82 pμ g · mL-1 and the correlation coefficient was 0.9992.The average recovery rate and relative standard deviation were 99.7% and RSD=0.96% （ n=5 ） .Conclusion ： This method is simple, accurate and reproducible, which can be used for quality control of Kangbingdu Mixture. |
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