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泽漆总黄酮的提取与含量测定
引用本文:牛明娟,惠秋沙. 泽漆总黄酮的提取与含量测定[J]. 齐鲁药事, 2013, 32(3): 131-133
作者姓名:牛明娟  惠秋沙
作者单位:牛明娟 (山东中医药大学,山东,济南,250355); 惠秋沙 (山东中医药大学,山东,济南,250355);
摘    要:目的探讨从泽漆中提取黄酮类成分的最佳方法,并对其含量进行测定。方法对泽漆黄酮的超声辅助提取工艺进行单因素和正交实验的研究。结果最佳提取工艺参数如下:醇浓度为60%,料液比为1∶25,超声时间为1 h,并且测得黄酮的含量为13.71 mg.g-1。结论此法的提取率高,简单准确,可用于泽漆的质量控制。

关 键 词:泽漆黄酮  提取  含量测定

Extraction and determination of helioscopia flavonoids
NIU Ming-juan,HUI Qiu-sha. Extraction and determination of helioscopia flavonoids[J]. qilu pharmaceutical affairs, 2013, 32(3): 131-133
Authors:NIU Ming-juan  HUI Qiu-sha
Affiliation:(Shandong University of Traditional Chinese Medicine,Jinan 250355,China)
Abstract:Objective To investigate the best extraction method of flavonoids from helioscopia,and to determine its content.Methods The ultrasonic-assisted extraction technology of helioscopia flavonoids was investigated by single factor and orthogonal design.Results The optimum extraction conditions were as follows:60% ethanol,liquid material ratio 1∶ 25 and ultrasonic 1 h.The content of flavonoid was 13.71 mg·g-1.Conclusion This method was simple,accurate with high extracting rate,and it can be used for the quality control of helioscopia.
Keywords:Helioscopia flavonoids  Extraction  Determination
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