| 银柴胡的化学成分 |
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| 引用本文： | 孙博航,吉川雅之,陈英杰,吴立军.银柴胡的化学成分[J].沈阳药科大学学报,2006,23(2):84-87. |
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| 作者姓名： | 孙博航 吉川雅之 陈英杰 吴立军 |
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| 作者单位： | 1. 沈阳药科大学,中药学院,辽宁,沈阳,110016
2. 日本京都药科大学,生药学教研室,日本国,京都,607-8412 |
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| 摘 要： | 目的对石竹科植物银柴胡(Stellaria dichatomaL.var.lanceolataBge.)干燥根银柴胡提取物的化学成分进行分离和结构鉴定。方法银柴胡的乙醇提取物经过氯仿正丁醇水萃取,正反相硅胶柱色谱和HPLC分离,最终分离得到10个化合物,应用核磁共振技术鉴定了其结构。结果10个化合物分别被鉴定为5羟甲基糠醛(5(hydroxymethyl)2 furfural,Ⅰ)、5羟甲基2甲酰基吡咯(5(hydroxymethyl)2 formyl pyrrole,Ⅱ)、香草醛(vanillin,Ⅲ)、香草酸(vanillic acid,Ⅳ)、1(4羟基3甲氧基苯基)乙酮(1(4 hydroxy 3 methoxyphenyl)ethanone,Ⅴ)、1(3′甲氧基4′5′甲叉基二氧)苯基丙醇(1 hydroxy 1(3′methoxy 4′5′methylenedioxy)phenylpropanol,Ⅵ)、二氢阿魏酸(dihydroferulic acid,Ⅶ)、3,4二甲氧基苯丙烯酸(3,4 dimethoxycinnamic acid,Ⅷ)、7烯豆甾醇3棕榈酸酯(stigmast 7 en 3 ol palmitate,Ⅸ)、5,7二羟基二氢黄酮(pinocembrin,Ⅹ)。结论化合物Ⅰ、Ⅲ~Ⅷ、Ⅹ为首次从该属植物中分离得到。
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| 关 键 词： | 银柴胡 化学成分 结构鉴定 |
| 文章编号： | 1006-2858(2006)02-0084-04 |
| 收稿时间： | 2004-12-01 |
| 修稿时间： | 2004年12月1日 |
Chemical contituents of Stellaria dichatoma L.var.lanceolata Bge. |
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| SUN Bo-hang,Yashikawa,CHEN Ying-jie,WU Li-jun.Chemical contituents of Stellaria dichatoma L.var.lanceolata Bge.[J].Journal of Shenyang Pharmaceutical University,2006,23(2):84-87. |
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| Authors: | SUN Bo-hang Yashikawa CHEN Ying-jie WU Li-jun |
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| Institution: | 1. School of Traditional Chinese Materia Medica, Shenyang Pharmaceutical University, Shenyang 110016, China ; 2. Kyoto Pharmaceutical University Shoyaku School, Kyoto, Japan, 607-8412 |
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| Abstract: | Objective To study the chemical constituents of Stellaria dichatoma L.var.lanceolata Bge.Methods The extract was extracted with CHCl_3,n-BuOH and H_2O,then isolated with normal and reflect-phase silica gel and HPLC.Results Ten compounds were identified as 5-(hydroxymethyl)-2furfural(Ⅰ),5-(hydroxymethyl)pyrrole-2-carboxaldehyde(Ⅱ),vanillin(Ⅲ),vanillic acid(Ⅳ),1-(4-hydroxy-3-methoxyphenyl)ethanone(Ⅴ),1-hydroxy-1-(3′methoxy-4′5′-methylenedioxy)phenylpropane(Ⅵ),dihydroferulic acid(Ⅶ),3,4-dimethoxy-hydrocinnamic acid(Ⅷ),stigmast-7-en-3-ol-palmitate(Ⅸ),pinacembrin(Ⅹ).Conclusions CompoundsⅠ,Ⅲ-Ⅷ,Ⅹ are isolated from Stellaria L.plants for the first time. |
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| Keywords: | Stellaria dichatoma L var lanceolata Bge chemical constituent structure dentification |
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