| 应用均匀设计研究2-甲基-5-巯基-1,3,4-噻二唑制备工艺 |
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| 引用本文： | 王旭,李敬芬,周淑晶,周天明. 应用均匀设计研究2-甲基-5-巯基-1,3,4-噻二唑制备工艺[J]. 中国现代应用药学, 1998, 15(2): 32-33 |
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| 作者姓名： | 王旭 李敬芬 周淑晶 周天明 |
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| 作者单位： | 佳木斯医学院药学系 |
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| 基金项目： | 湖北工学院校科研和教改项目，， |
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| 摘 要： | 应用均匀设计于标题化合物工艺研究中,以乙酸乙酯和水合肼于二甲苯中反应,加入CS_2,直接加热,一步环合成标题化合物,总收率达75.5％。
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| 关 键 词： | 均匀设计 2-甲基-5-巯基-1 3 4-噻二唑 制备 |
| 修稿时间： | 1997-03-14 |
Investigation of preparation of 2-Methyl-5-Mercapto-1,3,4-Thiadiazole with uniform design |
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| Wang Xu. Investigation of preparation of 2-Methyl-5-Mercapto-1,3,4-Thiadiazole with uniform design[J]. The Chinese Journal of Modern Applied Pharmacy, 1998, 15(2): 32-33 |
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| Authors: | Wang Xu |
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| Abstract: | The uniform design was applied to technological study of the title compound, starting from ethyl acetate and diamine hydrate,followed by reaction with carbon disulfide,the title compound was synthesized in one step.The overall yield amounts to 75.5% . |
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| Keywords: | uniform desing 2-methyl-5-mercapto-1 3 4-thiadiazole praparation |
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