| 回春酒质量标准的研究 |
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| 引用本文： | 蔡步林,郑金凤,李文莉. 回春酒质量标准的研究[J]. 中国药师, 2012, 15(9): 1241-1243 |
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| 作者姓名： | 蔡步林 郑金凤 李文莉 |
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| 作者单位： | 湖南省食品药品检验研究院,长沙,410000 |
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| 基金项目： | 国家药典委员会国家药品标准提高行动计划项目（编号：153） |
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| 摘 要： | 目的:建立回春酒质量标准。方法:采用TLC法对当归与丁香进行鉴别;用HPLC法测定淫羊藿的含量,色谱柱为Agilent TC-C18(250 mm×4.6 mm,5μm),流动相为乙腈-水(27∶73),柱温35℃,流速为0.8 ml.min-1,检测波长为270 nm。结果:TLC色谱斑点清晰;淫羊藿苷对照品在12.99～1 299 ng范围内线性关系良好(r=0.999 9),平均回收率为98.5%,RSD为1.5%(n=9)。结论:本法简便、可靠、准确,可用于该制剂的质量控制。
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| 关 键 词： | 回春酒 质量标准 薄层色谱法 高效液相色谱法 |
| 收稿时间： | 2012-04-16 |
| 修稿时间： | 2012-05-28 |
Study on the Quality Standard for Huichun Spirits |
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| Cai Bulin,Zheng Jinfeng and Li Wenli. Study on the Quality Standard for Huichun Spirits[J]. China Pharmacist, 2012, 15(9): 1241-1243 |
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| Authors: | Cai Bulin Zheng Jinfeng Li Wenli |
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| Affiliation: | (Hunan Institute for Food and Drug Control,Changsha 410000,China) |
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| Abstract: | Objective： To establish the quality standard for Huichun spirits.Method： Angelicae Sinensis Radix,Caryophylli Flos and Epimedii Folium in the spirits were identified by TLC.An Agilent TC-C18（250 mm×4.6 mm,5 μm） column was eluted with the mobile phase consisted of acetonitrile-water（27∶ 73） at the column temperature of 35℃.The flow rate was 0.8 ml·min-1 and detection wavelength was 270 nm.Result： The TLC spots were quite clear.The linear range of gallic acid was within 12.99-1 299 ng（r=0.999 9）,the average recovery was 98.5% and RSD was 1.5%（n=9）.Conclusion： The method is simple,reliable and accurate,and can be used in the quality control of Huichun spirits. |
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| Keywords: | Huichun spirits Quality srandard TLC HPLC |
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