| HPLC测定醋艾炭间羟基安息香酸的含量 |
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| 引用本文： | 王永丽,尉小慧,赵森淼,刘伟,李思蒙,侴桂新,王峥涛. HPLC测定醋艾炭间羟基安息香酸的含量[J]. 中国实验方剂学杂志, 2013, 19(18): 78-81 |
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| 作者姓名： | 王永丽 尉小慧 赵森淼 刘伟 李思蒙 侴桂新 王峥涛 |
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| 作者单位： | 上海中医药大学中药研究所;中药标准化教育部重点实验室;中药新资源与 质量标准综合评价国家中医药管理局重点研究室;上海中药标准化研究中心 上海 201203;上海中医药大学中药研究所;中药标准化教育部重点实验室;中药新资源与 质量标准综合评价国家中医药管理局重点研究室;上海中药标准化研究中心 上海 201203;上海中医药大学中药研究所;中药标准化教育部重点实验室;中药新资源与 质量标准综合评价国家中医药管理局重点研究室;上海中药标准化研究中心 上海 201203;上海中医药大学中药研究所;中药标准化教育部重点实验室;中药新资源与 质量标准综合评价国家中医药管理局重点研究室;上海中药标准化研究中心 上海 201203;上海中医药大学中药研究所;中药标准化教育部重点实验室;中药新资源与 质量标准综合评价国家中医药管理局重点研究室;上海中药标准化研究中心 上海 201203;上海中医药大学中药研究所;中药标准化教育部重点实验室;中药新资源与 质量标准综合评价国家中医药管理局重点研究室;上海中药标准化研究中心 上海 201203;上海中医药大学中药研究所;中药标准化教育部重点实验室;中药新资源与 质量标准综合评价国家中医药管理局重点研究室;上海中药标准化研究中心 上海 201203 |
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| 基金项目： | 国家药品标准提高研究项目(778) |
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| 摘 要： | 目的: 对不同产地醋艾炭间羟基安息香酸的含量进行比较研究,为醋艾炭的质量控制及合理利用提供科学依据。方法: 采用HPLC,Prevail C18色谱柱(4.6 mm×250 mm,5 μm),流动相乙腈-0.1%磷酸(15:85),流速1.0 mL·min-1,检 测波长240 nm,柱温25 ℃。结果: 间羟基安息香酸在0.010 02~0.501 00 μg具有良好的线性(r=1.000 0),平均回收率(n=9) 97.39%,RSD 0.99%。结论: 所建方法准确、简单、重复性好,不同产地醋艾炭间羟基安息香酸的含量差异显著。
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| 关 键 词： | 醋艾炭 高效液相色谱 间羟基安息香酸 |
| 收稿时间： | 2013-03-14 |
Content Determination of 3-Hydroxybenzoic Acid in Artemisiae Argyi Folium (Carbonized and Processed with Vinegar) by HPLC |
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| WANG Yong-li,WEI Xiao-hui,ZHAO Sen-miao,LIU Wei,LI Si-meng,CHOU Gui-xin and WANG Zheng-tao. Content Determination of 3-Hydroxybenzoic Acid in Artemisiae Argyi Folium (Carbonized and Processed with Vinegar) by HPLC[J]. China Journal of Experimental Traditional Medical Formulae, 2013, 19(18): 78-81 |
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| Authors: | WANG Yong-li WEI Xiao-hui ZHAO Sen-miao LIU Wei LI Si-meng CHOU Gui-xin WANG Zheng-tao |
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| Affiliation: | Institute of Chinese Materia Medica, Shanghai University of Traditional Chinese Medicine; the MOE Key Laboratory for Standardization of Chinese Medicines and the SATCM Key Laboratory for New Resources and Quality Evaluation of Chinese Medicines; Shanghai R&D Centre for Standardization of Chinese Medicines, Shanghai 201203, China;Institute of Chinese Materia Medica, Shanghai University of Traditional Chinese Medicine; the MOE Key Laboratory for Standardization of Chinese Medicines and the SATCM Key Laboratory for New Resources and Quality Evaluation of Chinese Medicines; Shanghai R&D Centre for Standardization of Chinese Medicines, Shanghai 201203, China;Institute of Chinese Materia Medica, Shanghai University of Traditional Chinese Medicine; the MOE Key Laboratory for Standardization of Chinese Medicines and the SATCM Key Laboratory for New Resources and Quality Evaluation of Chinese Medicines; Shanghai R&D Centre for Standardization of Chinese Medicines, Shanghai 201203, China;Institute of Chinese Materia Medica, Shanghai University of Traditional Chinese Medicine; the MOE Key Laboratory for Standardization of Chinese Medicines and the SATCM Key Laboratory for New Resources and Quality Evaluation of Chinese Medicines; Shanghai R&D Centre for Standardization of Chinese Medicines, Shanghai 201203, China;Institute of Chinese Materia Medica, Shanghai University of Traditional Chinese Medicine; the MOE Key Laboratory for Standardization of Chinese Medicines and the SATCM Key Laboratory for New Resources and Quality Evaluation of Chinese Medicines; Shanghai R&D Centre for Standardization of Chinese Medicines, Shanghai 201203, China;Institute of Chinese Materia Medica, Shanghai University of Traditional Chinese Medicine; the MOE Key Laboratory for Standardization of Chinese Medicines and the SATCM Key Laboratory for New Resources and Quality Evaluation of Chinese Medicines; Shanghai R&D Centre for Standardization of Chinese Medicines, Shanghai 201203, China;Institute of Chinese Materia Medica, Shanghai University of Traditional Chinese Medicine; the MOE Key Laboratory for Standardization of Chinese Medicines and the SATCM Key Laboratory for New Resources and Quality Evaluation of Chinese Medicines; Shanghai R&D Centre for Standardization of Chinese Medicines, Shanghai 201203, China |
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| Abstract: | |
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| Keywords: | Artemisiae Argyi Folium (carbonized and processed with vinegar) HPLC 3-hydroxybenzoic acid |
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