| GC法测定喉疾灵片中冰片含量的方法研究 |
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| 引用本文： | 汪剑飞.GC法测定喉疾灵片中冰片含量的方法研究[J].安徽医药,2011,15(11):1358-1359. |
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| 作者姓名： | 汪剑飞 |
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| 作者单位： | 安徽省芜湖市食品药品检验所,安徽,芜湖,241001 |
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| 摘 要： | 目的建立GC法测定喉疾灵片中冰片的含量测定方法。方法采用Rtx-50毛细管柱(30 m×0.25 mm,0.25μm),载气为氮气,FID检测器,柱温为恒温130℃,内标法测定冰片含量。结果冰片在0.405 4～2.027 0 g.L-1范围内浓度与峰面积呈良好的线性关系(r=0.999 0,n=5),平均加样回收率为99.21%,RSD为0.81%(n=9)。结论该方法快速、灵敏、结果准确,适用于喉疾灵片中冰片的含量测定。
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| 关 键 词： | GC法 喉疾灵片 冰片 |
Determination of Borneol in Houjiling Tablets by GC |
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| WANG Jian-fei.Determination of Borneol in Houjiling Tablets by GC[J].Anhui Medical and Pharmaceutical Journal,2011,15(11):1358-1359. |
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| Authors: | WANG Jian-fei |
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| Institution: | WANG Jian-fei(Wuhu Institute for Food ＆ Drug Control,Wuhu 241001) |
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| Abstract: | Aim To establish a GC method for the determination of Borneol in Houjiling tablets.Methods The Rtx-50 capillary column（30 m×0.25 mm,0.25 μm） was used with FID,nitrogen as the carrier gas,column temperature at 130 ℃.The internal standard method was used to determine the content of borneol.Results The borneol sample showed a good linear relationship at the range of 0.405 4~2.027 0 g·L-1（r=0.999 0,n=5）.The average recovery rate was 99.21% and RSD was 0.81%（n=9）.Conclusion This method is simple and accurate and able to determine of Borneol in Houjiling Tablets. |
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| Keywords: | GC Houjiling Tablets Borneol |
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