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三种方法提取防风挥发油的气质联用成分分析
引用本文:夏伦祝,彭代银,汪永忠,李毛全,章俊如,段贤春.三种方法提取防风挥发油的气质联用成分分析[J].安徽医药,2009,13(8):885-886.
作者姓名:夏伦祝  彭代银  汪永忠  李毛全  章俊如  段贤春
作者单位:安徽中医学院第一附属医院药学部;安徽中医学院·安徽省中药研究与开发重点实验室,安徽,合肥,230038
摘    要:目的对3种不同方法提取的防风挥发油化学成分进行分析。方法采用水蒸气蒸馏法(SD)、溶剂提取法(SX)、超临界CO2流体萃取法(SFE-CO2)提取防风挥发油,用气相-质谱(GC-MS)法对化学成分进行鉴定。结果水蒸气蒸馏法提取挥发油共鉴定了13种化学成分;溶剂提取法提取的挥发油共鉴定了18种化学成分;超临界CO2流体萃取法提取的挥发油共鉴定了21种化学成分。结论超临界CO2流体萃取法提取的挥发油更全面地反映药材中的化学成分。

关 键 词:防风  挥发油  GC-MS

GC-MS analysis of chemical constituents of the essential oil from saposhnikovia divaricata by three extraction methods
XIA Lun-zhu,Peng Dai-yin,WANG Yong-zhong,LI Mao-quan,ZHANG Jun-ru,DUAN Xian-chun.GC-MS analysis of chemical constituents of the essential oil from saposhnikovia divaricata by three extraction methods[J].Anhui Medical and Pharmaceutical Journal,2009,13(8):885-886.
Authors:XIA Lun-zhu  Peng Dai-yin  WANG Yong-zhong  LI Mao-quan  ZHANG Jun-ru  DUAN Xian-chun
Institution:XIA Lun-zhu1,Peng Dai-yin2,WANG Yong-zhong1,LI Mao-quan2,ZHANG Jun-ru1,DUAN Xian-chun1 (1.Division of Pharmac,First Affiliated Hospital of Anhui College of Traditional Chinese Medicine,2.Anhui College of Traditional Chinese Medicine,Anhui Key Laboratory of Chinese Medicine Research , Development,Hefei,Anhui 230038)
Abstract:Aim To analyze the chemical constituents of volatile oils from Saposhnikovia divaricata with three kinds of extraction methods.Method The essential oils were extracted from Saposhnikovia divaricata by supercritical fluid extraction(SFE)and steam distillation(SD).The amount of the components from the essential oil were determined by GC-MS.Results There were components from Saposhnikovia divaricata by SD that composed of about 13 of the total essential oil were extracted;There were components from Saposhnikov...
Keywords:GC-MS
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