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椒目超临界二氧化碳萃取物的分析
引用本文:李迎春,曾健青,刘莉玫,金雪松. 椒目超临界二氧化碳萃取物的分析[J]. 中药材, 2001, 24(7): 493-494
作者姓名:李迎春  曾健青  刘莉玫  金雪松
作者单位:1. 中国科学院广州化学研究所,
2. 南通华安超临界萃取有限公司,
摘    要:用气相色谱-质谱-计算机联用技术分析了椒目超临界CO_2萃取物,分离出59个组分,鉴定出其中35种化合物,占出峰总面积的96.22%。分析结果表明,超临界CO_2萃取椒目所得产物的化学成分中,脂肪酸及其酯类化合物占出峰物质总含量的90.83%,而单萜、倍半萜及其含氧衍生物仅占4.03%。萃取产物中含量最高的成分依次为油酸(38.91%)、棕榈酸(29.45%)、亚油酸甲酯(10.80%)和亚麻酸甲酯(8.64%)。

关 键 词:椒目  超临界CO_2萃取  气相色谱-质谱法
修稿时间:2001-04-17

GC-MS Analysis of Supercritical Carbon Dioxide Extraetfrom Seeds of Zanthoxylum bungeanun Maxim.
Li Yingchun,Zeng Jianqing,Liu Limei. GC-MS Analysis of Supercritical Carbon Dioxide Extraetfrom Seeds of Zanthoxylum bungeanun Maxim.[J]. Journal of Chinese medicinal materials, 2001, 24(7): 493-494
Authors:Li Yingchun  Zeng Jianqing  Liu Limei
Affiliation:Guangzhou Institute of Chemistry, Chinese Academy of Science, Guangzhou 510650.
Abstract:The chemical components of supercritical carbon dioxide extracts from seeds of Zanthoxylum bungeanun Maxim. were studied by GC-MS-DS.Thirty-five compounds which account for 96.22% of the total area of the chromatographic peaks , were identified.The results showed that fatty acids and esters occupied 90.83%of total chromatographic efflux of the extracts.The main components of the extracts are oleic acid(38.91%),palmitic acid (29.45%),linoleic acid methyl ester(10.80%),linolenic acid methyl ester(8.64%),et al.
Keywords:Seeds of Zanthoxylum bungeanun Maxim  Supercritical carbon dioxide extraction  GC-MS-DS
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