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| HPLC法测定抗病毒口服液中连翘苷的含量 | |
| 引用本文： | 赵辉,赵予,宫彦民,王宏志.HPLC法测定抗病毒口服液中连翘苷的含量[J].河南大学学报(医学版),2004,23(3):30-31. |
| 作者姓名： | 赵辉 赵予 宫彦民 王宏志 |
| 作者单位： | 1. 河南大学药学院,药物分析教研室,河南,开封,475001 2. 河南大学第一附属医院,药剂科,河南,开封,475001 3. 天津药业集团新郑股份有限公司,河南,新郑,451100 4. 河南省高等医药技工学校,河南,开封,475003 |
| 摘 要： | 目的 :以高效液相色谱法测定抗病毒口服液中连翘苷的含量。方法 :色谱条件 :ELITEC18色谱柱 ;流动相 :乙腈 -水 (2 5∶75 ) ;流速 :1.0ml/min ;检测波长 :2 77nm ;柱温 :室温。结果 :在 6份不同浓度下 ,测得平均回收率为10 1.4 5 % ,RSD为 2 .0 0 % ,稳定性与精密度分别为 1.4 %和 1.4 %。结论 :该方法简便 ,准确 ,可作为测定抗病毒口服液中连翘苷含量的方法 |
| 关 键 词： | 高效液相法 抗病毒口服液 连翘苷 |
| 文章编号： | 1672-7606(2004)03-0030-02 |
| 修稿时间： | 2004年3月25日 |
Determination of forsythin in Antivirus Oral Liquid by HPLC |
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| ZHAO Hui ,ZHAO Yu ,GONG Yan-min ,WANG Zhi-hong.Determination of forsythin in Antivirus Oral Liquid by HPLC[J].Journal of Henan University,2004,23(3):30-31. | |
| Authors: | ZHAO Hui ZHAO Yu GONG Yan-min WANG Zhi-hong |
| Institution: | ZHAO Hui 1,ZHAO Yu 2,GONG Yan-min 3,WANG Zhi-hong 4 |
| Abstract: | Objective: To determine the contents of forsythin in Antivirus oral liquid with HPLC. Methods: The reverse phase system of ELITE was C18 column ; the mobile phase was acetonitrile - water (25∶75) with a flow rate of 1.0ml/min ; the detection wavelength was 277nm; the column temperature was 10℃-30℃. Results: The average recovery rate at six different levels were 101.45% , RSD=2.00%. Stability and sophistication was respectively 1.4%and 1.4%. Conclusion: The method is simple and accurate, and can be used as the quality control of antitoxin oral liquid. |
| Keywords: | HPLC Antivirus Oral Liquid Forsythin |
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