| 黄连紫草凝胶质量标准 |
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| 引用本文： | 刘丽花,翟来超,陈天朝.黄连紫草凝胶质量标准[J].中国中医药现代远程教育,2014(22):111-113. |
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| 作者姓名： | 刘丽花 翟来超 陈天朝 |
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| 作者单位： | 河南中医学院第一附属医院药学部 |
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| 基金项目： | 河南中医学院院级课题[No:2008kj14] |
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| 摘 要： | 目的：建立黄连紫草凝胶的质量标准。方法采用TLC鉴别黄连紫草凝胶中的黄连、地黄、当归、紫草、黄柏；采用HPLC对制剂中的盐酸小檗碱进行含量测定。结果盐酸小檗碱在7.64~38.2μg＆#183;mL-1范围内线性良好，平均回收率100.38%， RSD3.79%。结论该方法简单易操作，结果准确可靠，重复性好，可作为黄连紫草凝胶的质量控制标准。
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| 关 键 词： | 黄连紫草凝胶 质量标准 高效液相色谱 薄层色谱 |
Rhizoma Coptidis Radix Arnebiae Seu Lithospermi Gel Quality Standards |
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| Liu Lihua;Zhai Laichao;Chen Tianchao.Rhizoma Coptidis Radix Arnebiae Seu Lithospermi Gel Quality Standards[J].Chinese Medicine Modern Distance Education of China,2014(22):111-113. |
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| Authors: | Liu Lihua;Zhai Laichao;Chen Tianchao |
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| Institution: | Liu Lihua;Zhai Laichao;Chen Tianchao;Pharmacy department, the first affiliated hospital of Henan college of TCM; |
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| Abstract: | Objective Establish the quality standards of rhizoma coptidis radix arnebiae seu lithospermi gel. Methods The TLC identifica-tion of rhizoma coptidis in rhizoma coptidis, radix rehmanniae, radix arnebiae seu lithospermi gel angelica, radix arnebiae seu lithospermi, cortex phellodendri; Content of the preparation of berberine hydrochloride by HPLC determination. Results Berberine hydrochloride in 7.64~38.2μg＆#183;mL-1 within the scope of linear is good, the average recovery of 100.38%, RSD3.79%. Conclusion The method is simple and easy to operate, reliable results are accurate and good repeatability can be used as the quality control of rhizoma coptidis radix arnebiae seu lithospermi gel. |
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| Keywords: | Rhizoma coptidis radix arnebiae seu lithospermi gel quality standards HPLC thin layer chromatography |
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