正交设计优选跌打促愈片中挥发油的提取工艺 |
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引用本文: | 张春林,;陈卫红,;蒋孟良,;彭聪,;李有兰.正交设计优选跌打促愈片中挥发油的提取工艺[J].中医药导报,2014(6):80-82. |
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作者姓名: | 张春林 ;陈卫红 ;蒋孟良 ;彭聪 ;李有兰 |
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作者单位: | [1]河南省洛阳正骨医院,河南洛阳471013; [2]湖南中医药大学第二附属医院,湖南长沙410005; [3]湖南中医药大学,湖南长沙410208; [4]湖南中医药大学药学院,湖南长沙410208 |
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基金项目: | 湖南省科技厅科技计划资助项目(No.2013SK3104) |
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摘 要: | 目的:优选倍他环糊精包合跌打促愈片中挥发油的最佳工艺。方法:采用L9(34)正交试验,以挥发油提取量为评价指标,优选其最佳提取工艺。结果:最佳工艺为:A2B3C3D2,即饮片粉碎成粗粒,加10倍量水,浸泡2 h,提取3 h。结论:优选的提取工艺合理而可行,可用于跌打促愈片中挥发油的提取。
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关 键 词: | 跌打促愈片 正交设计 挥发油 提取工艺 |
Study on Extraction Technology for Volatile Oil on Diedacuyu Tablet |
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Institution: | ZHANG Chun-lin, CHEN Wei-hon(Corresponding Author), JIANG Meng-liang, PENG Cong, LI You-lan (1. Luoyang Orthopedic-Traumatological Hospital, Luoyang He'nan 471013; 2. The Second Affiliated Hospital of Hunan University of Chinese Medicine, Changsha Hunan 410005; 3. Hunan University of Chinese Medicine, Changsha Hunan 410208; 4. College of Pharmacy, Hunan University of Chinese Medicine, Changsha Hunan 410208) |
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Abstract: | Objective: To study optimum extraction process conditions for volatile oil in Diedacuyu Tablet. Methods: The L9 (34) orthogonal test was used on optimizing the best process to the quantity of volatile oil as the evaluation index. Results: The optimum preparation conditions for extraction were established as A2B3C3D2 decoction pieces crushed into coarse grain, soaking for 2 h, extracting for 3.0 h with 10 times amount of water. Conclusion: This process is reasonable and feasible, and can be used for the extract of the volatile oil from Diedacuyu Tablet. |
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Keywords: | Diedacuyu Tablet Orthogonal design Volatile oil Extraction process |
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