| HPLC法测定蜂胶片中芦丁的含量 |
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| 引用本文： | 陶俊钰,鲍恩泉,秦绍刚,王玮.HPLC法测定蜂胶片中芦丁的含量[J].安徽医药,2008,12(6):505-506. |
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| 作者姓名： | 陶俊钰 鲍恩泉 秦绍刚 王玮 |
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| 作者单位： | 安徽省巢湖市药品检验所,安徽,巢湖,238000;安徽省巢湖市药品检验所,安徽,巢湖,238000;安徽省巢湖市药品检验所,安徽,巢湖,238000;安徽省巢湖市药品检验所,安徽,巢湖,238000 |
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| 摘 要： | 目的HPLC法测定蜂胶片中芦丁的含量。方法采用十八烷基硅烷键合硅胶柱；流动组成：0．4％磷酸水溶液．甲醇．乙腈（60：45：5），检测波长为256nm；流速为1．0ml·min^-1。结果芦丁线性范围为0．2603-1．5618μg，平均回收率为98．6％，RSD=1．86％（n=5）。结论方法简便可靠，结果准确。能有效控制蜂胶片的质量。
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| 关 键 词： | 蜂胶片 芦丁 |
| 修稿时间： | 2007年12月25 |
Determination of rutin in the proplis tablets by HPLC |
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| TAO Jun-yu,BAO En-quan,QIN Shao-gang,WANG Wei.Determination of rutin in the proplis tablets by HPLC[J].Anhui Medical and Pharmaceutical Journal,2008,12(6):505-506. |
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| Authors: | TAO Jun-yu BAO En-quan QIN Shao-gang WANG Wei |
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| Institution: | ( Chaohu Institute for Drug Control, Chaohu 238000, China) |
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| Abstract: | Aim To determine rutin in the proplis tablets by HPLC. Methods The octadecyl silicon hydride linkage silica gel column was used and methyl 0. 4% phosphoric acid-methanol-acetonitrile （60： 45： 5） was used as mobile phase. The detective wavelength was at 256 nm and the speed of flow is 1.0 ml · min^-1. Results The linear range for rutin is between 0. 2603 μg and 1. 5618 μg. Average recovery for rutin was 98.6% with RSD of 1.86% （ n = 5）. Conclusion This method is proved to be simple, reliable and can be used for the effective quality control of proplis tablets. |
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| Keywords: | HPLC rutin proplis tablets |
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