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| 大孔吸附树脂法分离纯化当归中阿魏酸的工艺研究 | |
| 引用本文： | 金汝城,李贵文,马素丽. 大孔吸附树脂法分离纯化当归中阿魏酸的工艺研究[J]. 中草药, 2008, 39(9): 1324-1327 |
| 作者姓名： | 金汝城 李贵文 马素丽 |
| 作者单位： | 1. 兰州理工大学生命科学与工程学院,甘肃兰州,730050 2. 兰州理工大学石油化工学院,甘肃,兰州,730050 3. 兰州理工大学理学院,甘肃,兰州,730050 |
| 摘 要： | 目的选择较合适的大孔吸附树脂,对当归中阿魏酸进行富集纯化,提高产品质量。方法采用大孔吸附树脂对阿魏酸进行吸附及洗脱性能试验,同时采用HPLC法进行分析检测。结果筛选出较合适的吸附树脂DA201,得到了最佳的工艺参数,使阿魏酸的质量分数由原材料中的0.15%富集提高到25.1%。结论该工艺成本低,效果好,树脂可重复使用,对于当归中阿魏酸的纯化有很好的应用前景。 |
| 关 键 词： | 当归 阿魏酸 大孔吸附树脂 高效液相色谱 |
| 收稿时间： | 2007-12-01 |
Separation and purification technology of ferulic acid in Angelica sinensis by macroporous adsorption resin |
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| JIN Ru-cheng,LI Gui-wen and MA Su-li. Separation and purification technology of ferulic acid in Angelica sinensis by macroporous adsorption resin[J]. Chinese Traditional and Herbal Drugs, 2008, 39(9): 1324-1327 | |
| Authors: | JIN Ru-cheng LI Gui-wen MA Su-li |
| Affiliation: | School of Life Science and Technology, Lanzhou University of Technology, Lanzhou 730050, China;School of Petrochemical Technology, Lanzhou University of Technology, Lanzhou 730050, China;School of Science, Lanzhou University of Technology, Lanzhou 730050, China |
| Abstract: | Objective To select the suitable macroporous adsorption resins for enrichment and purifi-cation ferulic acid from Angelica sinensis so as to improve the product quality. Methods Macroporous ad-sorption resins were used to study the adsorption and desorption characteristics of ferulic acid. At the same time HPLC was used in detection. Results The best resin DA201 was chosen and the optimum parameters were obtained. The content of ferulic acid was increased from 0. 15% in the raw material to 25.1%. Con-clusion The material has a low cost and the operation is easy. The adsorption resins can be used again,which has a good applied foreground. |
| Keywords: | Angelica sinensis (Oliv. ) Diels ferulic acid macroporous adsorption resin HPLC |
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