| 瓦楞子的炮制工艺优选 |
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| 引用本文： | 陶明宝,鄢玉芬,陈林,刘友平,尹科磊,陈鸿平. 瓦楞子的炮制工艺优选[J]. 中国实验方剂学杂志, 2017, 23(21): 24-29 |
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| 作者姓名： | 陶明宝 鄢玉芬 陈林 刘友平 尹科磊 陈鸿平 |
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| 作者单位： | 成都中医药大学 药学院, 中药材标准化教育部重点实验室, 四川省中药资源系统研究与开发利用重点实验室——省部共建国家重点实验室培育基地, 成都 611137,成都中医药大学 药学院, 中药材标准化教育部重点实验室, 四川省中药资源系统研究与开发利用重点实验室——省部共建国家重点实验室培育基地, 成都 611137,成都中医药大学 药学院, 中药材标准化教育部重点实验室, 四川省中药资源系统研究与开发利用重点实验室——省部共建国家重点实验室培育基地, 成都 611137,成都中医药大学 药学院, 中药材标准化教育部重点实验室, 四川省中药资源系统研究与开发利用重点实验室——省部共建国家重点实验室培育基地, 成都 611137,成都中医药大学 药学院, 中药材标准化教育部重点实验室, 四川省中药资源系统研究与开发利用重点实验室——省部共建国家重点实验室培育基地, 成都 611137,成都中医药大学 药学院, 中药材标准化教育部重点实验室, 四川省中药资源系统研究与开发利用重点实验室——省部共建国家重点实验室培育基地, 成都 611137 |
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| 基金项目： | 《全国中药饮片炮制规范》研究项目（2015-YP-48） |
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| 摘 要： | 目的:优选瓦楞子的炮制工艺,为控制瓦楞子炮制品的质量奠定基础。方法:以性状、饮片得率、水溶性浸出物含量、水煎液Ca2+含量和水浸液p H的综合评分为指标,通过单因素试验和正交试验优选瓦楞子煅制工艺和煅醋淬工艺,并与其煅制后盐水淬工艺、水淬工艺进行比较。结果:瓦楞子最佳煅制工艺条件为温度750℃,煅制时间30 min;最佳煅醋淬工艺条件为温度850℃,煅制90 min后立即投入0.3倍量醋浓度为9%的米醋中进行醋淬,至醋吸净为度;不同炮制工艺多指标综合评分的排序为煅醋淬品煅制品煅盐水淬品煅水淬品;最优工艺条件下煅醋淬品的性状符合"灰白色,质地酥脆"的要求,其饮片得率67.40%,p H 12.47,水溶性浸出物质量分数9.70%,水煎液Ca2+质量分数7.01%。结论:优选的炮制工艺稳定可行,可指导今后工业化生产,提高瓦楞子炮制品的质量,确保临床用药的安全性和有效性。
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| 关 键 词： | 瓦楞子 炮制工艺 煅制 煅醋淬 综合评分 水溶性浸出物 钙离子 |
| 收稿时间： | 2017-05-06 |
Optimization of Processing Technology of Arcae Concha |
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| TAO Ming-bao,YAN Yu-fen,CHEN Lin,LIU You-ping,YIN Ke-lei and CHEN Hong-ping. Optimization of Processing Technology of Arcae Concha[J]. China Journal of Experimental Traditional Medical Formulae, 2017, 23(21): 24-29 |
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| Authors: | TAO Ming-bao YAN Yu-fen CHEN Lin LIU You-ping YIN Ke-lei CHEN Hong-ping |
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| Affiliation: | Pharmacy College, Chengdu University of Traditional Chinese Medicine, Key Laboratory of Standardization of Chinese Herbal Medicine, Ministry of Education, Key Laboratory of Systematic Research, Development and Utilization of Chinese Medicine Resources in Sichuan Province, Key Laboratory Breeding Base of Co-founded by Sichuan Province and Ministry of Science and Technology, Chengdu 611137, China,Pharmacy College, Chengdu University of Traditional Chinese Medicine, Key Laboratory of Standardization of Chinese Herbal Medicine, Ministry of Education, Key Laboratory of Systematic Research, Development and Utilization of Chinese Medicine Resources in Sichuan Province, Key Laboratory Breeding Base of Co-founded by Sichuan Province and Ministry of Science and Technology, Chengdu 611137, China,Pharmacy College, Chengdu University of Traditional Chinese Medicine, Key Laboratory of Standardization of Chinese Herbal Medicine, Ministry of Education, Key Laboratory of Systematic Research, Development and Utilization of Chinese Medicine Resources in Sichuan Province, Key Laboratory Breeding Base of Co-founded by Sichuan Province and Ministry of Science and Technology, Chengdu 611137, China,Pharmacy College, Chengdu University of Traditional Chinese Medicine, Key Laboratory of Standardization of Chinese Herbal Medicine, Ministry of Education, Key Laboratory of Systematic Research, Development and Utilization of Chinese Medicine Resources in Sichuan Province, Key Laboratory Breeding Base of Co-founded by Sichuan Province and Ministry of Science and Technology, Chengdu 611137, China,Pharmacy College, Chengdu University of Traditional Chinese Medicine, Key Laboratory of Standardization of Chinese Herbal Medicine, Ministry of Education, Key Laboratory of Systematic Research, Development and Utilization of Chinese Medicine Resources in Sichuan Province, Key Laboratory Breeding Base of Co-founded by Sichuan Province and Ministry of Science and Technology, Chengdu 611137, China and Pharmacy College, Chengdu University of Traditional Chinese Medicine, Key Laboratory of Standardization of Chinese Herbal Medicine, Ministry of Education, Key Laboratory of Systematic Research, Development and Utilization of Chinese Medicine Resources in Sichuan Province, Key Laboratory Breeding Base of Co-founded by Sichuan Province and Ministry of Science and Technology, Chengdu 611137, China |
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| Abstract: | |
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| Keywords: | Arcae Concha processing technology calcining calcined vinegar comprehensive score water soluble extract Ca2+ |
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