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Simple Preparation of Novel Metal-Containing Mesoporous Starches
Authors:Manuel Ojeda  Vitaliy Budarin  Peter S. Shuttleworth  James H. Clark  Antonio Pineda  Alina M. Balu  Antonio A. Romero  Rafael Luque
Abstract:Metal-containing mesoporous starches have been synthesized using a simple and efficient microwave-assisted methodology followed by metal impregnation in the porous gel network. Final materials exhibited surface areas >60 m2 g−1, being essentially mesoporous with pore sizes in the 10–15 nm range with some developed inter-particular mesoporosity. These materials characterized by several techniques including XRD, SEM, TG/DTA and DRIFTs may find promising catalytic applications due to the presence of (hydr)oxides in their composition.
Keywords:mesoporous polysaccharides   starch   Fe   Co   Cu
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