| 寒喘祖帕颗粒的质量标准研究 |
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| 引用本文： | 金晓红,桂红武,耿伟. 寒喘祖帕颗粒的质量标准研究[J]. 中国药房, 2012, 0(15): 1405-1406 |
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| 作者姓名： | 金晓红 桂红武 耿伟 |
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| 作者单位： | [1]诸暨市人民医院药剂科,浙江诸暨311800 [2]新疆维吾尔自治区人民医院北院,乌鲁木齐830054 [3]新疆医科大学第一附属医院药学部,乌鲁木齐830054 |
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| 摘 要： | 目的:建立寒喘祖帕颗粒的质量标准。方法:采用薄层色谱(TLC)法对制剂中玫瑰花、小茴香进行定性鉴别;采用高效液相色谱法对制剂中甘草酸铵进行含量测定。结果:TCL斑点清晰、重复性好;甘草酸铵检测浓度在20.62～206.2μg.mL-1范围内与峰面积积分值呈良好线性关系(r=0.9998),平均回收率为100.21%,RSD=1.52%(n=9)。结论:所建标准可用于寒喘祖帕颗粒的质量控制。
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| 关 键 词： | 寒喘祖帕颗粒 薄层色谱法 甘草酸铵 高效液相色谱法 |
Study on the Quality Standard of Hanchuan Zupa Granules |
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| JIN Xiao-hongDept.of Pharmacy,Zhuji Municipal People＇s Hospital,Zhejiang Zhuji,China GUI Hong-wuNorth Branch,People＇s Hospital of Xinjiang Uygur Autonomous Region,Urumqi,China GENG Wei. Study on the Quality Standard of Hanchuan Zupa Granules[J]. China Pharmacy, 2012, 0(15): 1405-1406 |
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| Authors: | JIN Xiao-hongDept.of Pharmacy Zhuji Municipal People＇s Hospital Zhejiang Zhuji China GUI Hong-wuNorth Branch People＇s Hospital of Xinjiang Uygur Autonomous Region Urumqi China GENG Wei |
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| Affiliation: | JIN Xiao-hong(Dept.of Pharmacy,Zhuji Municipal People＇s Hospital,Zhejiang Zhuji 311800,China) GUI Hong-wu(North Branch,People＇s Hospital of Xinjiang Uygur Autonomous Region,Urumqi 830054,China) GENG Wei(Dept.of Pharmacy,The First Affiliated Hospital of Xinjiang Medical University,Urumqi 830054,China) |
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| Abstract: | OBJECTIVE：To establish the quality standard of Hanchuan zupa granules.METHODS：Rose rugosa and Fructus foeniculi were identified by TLC.The content of ammonium glycyrrhetate in the preparation was determined by HPLC.RESULTS：The TLC spots were clear and well-repeated.The linear range of ammonium glycyrrhetate was 20.62～206.2 μg·mL-1（r=0.999 8） with an average recovery of 100.21%（RSD=1.52%,n=9）.CONCLUSION：Established quality standard can be used for the quality control of Hanchuan zupa granules. |
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| Keywords: | Hanchuan zupa granules TLC Ammonium glycyrrhetate HPLC |
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