| 高效液相色谱-蒸发光散射检测器测定芦荟西洋参软胶囊中的芦荟苷和人参皂苷Rb1、Rg1和Re含量 |
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| 引用本文： | 宋明侠. 高效液相色谱-蒸发光散射检测器测定芦荟西洋参软胶囊中的芦荟苷和人参皂苷Rb1、Rg1和Re含量[J]. 按摩与康复医学, 2011, 0(3): 3-4 |
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| 作者姓名： | 宋明侠 |
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| 作者单位： | 山东临沂大学,临沂276005 |
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| 摘 要： | 建立了高效液相色谱法-蒸发光散射检测器法（HPLC-ELSD）测定芦荟西洋参软胶囊中芦荟苷和人参皂苷Rb1、Rg1和Re含量测定方法.C18柱;流动相为乙腈-水（22∶78,甲酸调pH.至2.2）;流速0.8mL/min;芦荟苷、人参皂苷Re、Rb1、Rg1在.2～1.2μg.ml-1的范围内呈良好的线性关系,回收率均在96.8～102.1%之间,RSD均低于3.6%;结果准确可靠,适用于该产品的质量控制.
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| 关 键 词： | 芦荟西洋参软胶囊 芦荟苷 人参皂苷Rb1 人参皂苷Rg1 人参皂苷Re |
In highly effective liquid chromatography - evaporation light scattering detector determination aloe American ginseng soft capsule aloe glucoside and ginseng soap glucoside Rb1,Rg1 and Re content |
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| Song Mingxia. In highly effective liquid chromatography - evaporation light scattering detector determination aloe American ginseng soft capsule aloe glucoside and ginseng soap glucoside Rb1,Rg1 and Re content[J]. Chinese Manipulation and Rehabilitation Medicine, 2011, 0(3): 3-4 |
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| Authors: | Song Mingxia |
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| Affiliation: | Song Mingxia |
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| Abstract: | Has established in the highly effective liquid phase chromatography - evaporation light scattering detector law （HPLC- ELSD） determination aloe American ginseng soft capsule the aloe glucoside and ginseng soap glucoside Rhl, Rgl and the Re content determi- nation method. Cl8 column;The flowing for second grade nitrile - water （22.. 78, formic acid adjusts pH. to 2.2）;Speed of flow 0. 8mL/ min;Aloe glucoside, ginseng soap glucoside Re, Rb1 , Rg1 in. 2- 1.2μg. rn1-1 scope assumes the good linear relations, the returns-ratio between 96.8-102. 1% ,RSD is lower than 3.6% ;Result accurate reliable,is suitable in this product quality control. |
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| Keywords: | Aloe American ginseng soft capsule Aloe glucoside Ginseng soap glucoside Rhl Ginseng soap glucoside Rgl Ginseng soap glucoside Re |
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