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| 羽芒菊化学成分研究 | |
| 引用本文： | 徐润生,袁珂,殷明文,方磊杰,毛浓浓. 羽芒菊化学成分研究[J]. 中草药, 2009, 40(7): 1015-1018 |
| 作者姓名： | 徐润生 袁珂 殷明文 方磊杰 毛浓浓 |
| 作者单位： | 1. 浙江林学院天然药物研发中心,浙江,临安,311300;浙江师范大学化学与生命科学学院,浙江,金华,321004 2. 浙江林学院天然药物研发中心,浙江,临安,311300 3. 郑州大学化学系,河南,郑州,450052 |
| 基金项目： | 浙江省森林培育重中之重学科开放基金 |
| 摘 要： | 目的 研究羽芒菊Tridax procumbens的化学成分.方法 利用Diaion HP-20、MCI-Gel CHP-20、Sepha-dex LH-20及硅胶等柱色谱法对羽芒菊中的化学成分进行分离纯化,根据理化性质和波谱技术(1H-NMR、13C-NMR、DEPT、1H-1H COSY、HSQC、HMBC、ESI-MS、IR)鉴定化合物的结构.结果 从中分离鉴定了5个化合物:8,3'-二羟基-3,7,4'-三甲氧基-6-O-β-D-葡萄糖黄酮苷-6"-乙酸酯(Ⅰ)、豆甾醇(Ⅱ)、β-谷甾醇(Ⅲ)、邻苯二甲酸二-(2-乙基)己酯(Ⅳ)、芹菜素-7-O-β-D-葡萄糖苷(Ⅴ).结论 化合物Ⅰ为新化合物,命名为羽芒菊苷A(trid-proeumoside A).化合物Ⅱ～Ⅴ为首次从该植物中分离得到. |
| 关 键 词： | 羽芒菊 化学成分 羽芒菊苷A |
| 收稿时间： | 2009-02-28 |
Chemical constituents in Tridax procumbens |
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| XU Run-sheng,YUAN Ke,YIN Ming-wen,FANG Lei-jie and MAO Nong-nong. Chemical constituents in Tridax procumbens[J]. Chinese Traditional and Herbal Drugs, 2009, 40(7): 1015-1018 | |
| Authors: | XU Run-sheng YUAN Ke YIN Ming-wen FANG Lei-jie MAO Nong-nong |
| Affiliation: | Research and Development Center of Natural Medicine,Zhejiang Forestry University,Lin'an 311300,China;College of Chemistry and Life Science,Zhejiang Normal University,Jinhua 321004,China;Research and Development Center of Natural Medicine,Zhejiang Forestry University,Lin'an 311300,China;Department of Chemistry,Zhengzhou University,Zhengzhou 450052,China;Research and Development Center of Natural Medicine,Zhejiang Forestry University,Lin'an 311300,China;Research and Development Center of Natural Medicine,Zhejiang Forestry University,Lin'an 311300,China |
| Abstract: | Objective To study the chemical constituents in Tridax procumbens from Hainan Province. Methods The constituents were separated and purified by column chromatography with macroporous ad-sorption resin Diaion HP-20, MCI Gel CHP-20, Sephadex LH-20, and normal phase silica gel. Their structures were identified on the basis of physiochemical properties and spectral methods (1H-NMR, 13C-NMR, DEPT, 1H-1H COSY, HSQC, HMBC, ESI-MS, and IR). Results Five compounds were iso-lated and identified as: 8, 3'-dihydroxy-3, 7, 4'-trimethoxy-6-O-β-D-flavone glycoside-6"-acetate (Ⅰ), stigmasterol (Ⅱ), β-sitosterol (Ⅲ), bis (2-ethylhexyl) phthalate (Ⅳ), apigenin-7-O-β-D-glucoside (Ⅴ).Conclusion Compound Ⅰ is a new compound, named tridprocumoside A, the other compounds are isola-ted from this plant for the first time. |
| Keywords: | Tridax procumbens L. chemical constituents tridprocumoside A |
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