| 高效液相色谱法测定鱼丙涂剂中丙酸睾酮的含量 |
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| 引用本文： | 邓代全,冯碧敏,张昊. 高效液相色谱法测定鱼丙涂剂中丙酸睾酮的含量[J]. 中国药房, 2006, 17(3): 213-214 |
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| 作者姓名： | 邓代全 冯碧敏 张昊 |
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| 作者单位： | 泸州医学院附属医院,泸州市,646000 |
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| 摘 要： | 目的建立以高效液相色谱法测定鱼丙涂剂中丙酸睾酮含量的方法。方法色谱柱为Kromasil C18,流动相为甲醇-水溶液(80∶20),检测波长为254nm,流速为1.0ml/min。结果丙酸睾酮检测浓度在100~400mg/ml范围内线性关系良好(r=0.9997);平均回收率为98.5%(RSD=0.55%)。结论本法简便、准确、重现性好,可用于鱼丙涂剂的质量控制。
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| 关 键 词： | 高效液相色谱法 鱼丙涂剂 丙酸睾酮 含量测定 |
| 文章编号： | 1001-0408(2006)03-0213-02 |
| 收稿时间： | 2005-04-19 |
| 修稿时间： | 2005-07-19 |
Content Determination of Testosterone Propionate in Testosterone Propionate Paints by HPLC |
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| DENG Daiquan,FENG Bimin,ZHANG Hao. Content Determination of Testosterone Propionate in Testosterone Propionate Paints by HPLC[J]. China Pharmacy, 2006, 17(3): 213-214 |
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| Authors: | DENG Daiquan FENG Bimin ZHANG Hao |
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| Affiliation: | The Affiliated Hospital of Luzhou Medical College, Luzhou 646000, China |
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| Abstract: | OBJECTIVE:To establish a HPLC method for the content determination of testosterone propionate in testosterone propionate paints.METHODS:The assaying was conducted on a Kromasil C 18 column with methanol-water solution(80∶20)as mobile phase,the detection wavelength was254nm and the flow rate was1.0ml/min.RESULTS:The linear concentration range of the testosterone propionate was100～400mg/ml(r=0.9997)with average recovery rate at98.5%(RSD=0.55%).CONCLUSION:The method is simple,accurate and reproducible,and it can be used for the quality control of testosterone propionate paints. |
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| Keywords: | HPLC Testosterone propionate paints Testosterone propionate Content determination |
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