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| 高效液相色谱法测定肾衰胶囊中游离大黄酚的含量 | |
| 引用本文： | 叶雪莹,申玉华,孙玉平,于文静,霍玉华.高效液相色谱法测定肾衰胶囊中游离大黄酚的含量[J].中国药品标准,2001,2(1):61-63. |
| 作者姓名： | 叶雪莹 申玉华 孙玉平 于文静 霍玉华 |
| 作者单位： | 1. 吉林省药品检验所,长春,130062 2. 浙江万马药业有限公司,杭州,310011 3. 德惠市药品检验所,长春 |
| 摘 要： | 目的：建立准确、稳定的含量测定方法，有效地控制制制剂质量。方法：以甲醇提取，HPLC法测定样品中游离大黄酚的含量。结果：样品中大黄酚得到较好分离。其加样回收率为98.67%，RSD为0.97%，结论：本法能有效地控制该制剂的质量。 |
| 关 键 词： | 高效液相色谱法 肾衰胶囊 大黄酚 含量 质量控制 |
DETERMINATION OF FREE CHRYSOPHANOL IN SHENSHUAICAPSULE BY HPLC |
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| Authors: | Ye Xueying Shen Yuhu Sun yuping Yu wenjing and Huo yuhua |
| Institution: | Jilin Institute for Drug Control, Changchun 130062;Jilin Institute for Drug Control, Changchun 130062;Jilin Institute for Drug Control, Changchun 130062;Jilin Institute for Drug Control, Changchun 130062;Jilin Institute for Drug Control, Changchun 130062 |
| Abstract: | Objective: Setting an accurate quantitative determination method to control the preparation quality. Method: Chrysophanol in preparation was extracted by methanol ,then was determined by HPLC. Result: The arerage recovery of the added index was 98. 67%,RSD was 0. 97%(n = 6). Conclusion: The quantitative determination method can be used for the quality control of Shenshuai Capsule. |
| Keywords: | HPLC Shenshuai Capsule Chrysophanol |
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