| 高效液相色谱法测定珍黄片的含量 |
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| 引用本文： | 白玉红,郑清娉,胡克菲. 高效液相色谱法测定珍黄片的含量[J]. 中国当代医药, 2009, 16(13): 134-135 |
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| 作者姓名： | 白玉红 郑清娉 胡克菲 |
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| 作者单位： | 1. 辽宁省营口药品检验所,辽宁营口,115001
2. 北京因科瑞斯生物制品研究所,北京,102209 |
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| 摘 要： | 目的：建立高效液相色谱法测定珍黄片的含量。方法：采用高效液相色谱法对制剂中人参皂苷Rg1、人参皂苷Rb1和三七皂苷R1的含量进行测定。结果：人参皂苷Rg1、人参皂苷Rb1和三七皂苷R1的线性范围分别为1．144～11．440μg（r=0．9999）、0．948～9．480μg（r=0．9999）和0．434-4．340μg（r=0．9998），平均回收率分别为96．46％（RSD=1．01％）、98．17％（RSD=1．02％）和96．27％（RSD=1．16％）。结论：该方法简便、灵敏、准确，适用于珍黄片的含量测定。
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| 关 键 词： | 珍黄片 含量测定 高效液相色谱 |
Simultaneous assay of Zhenhuang tablets by HPLC |
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| BAI Yuhong,ZHENG Qingping,HU Kefei. Simultaneous assay of Zhenhuang tablets by HPLC[J]. http://www.botanicus.org/, 2009, 16(13): 134-135 |
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| Authors: | BAI Yuhong ZHENG Qingping HU Kefei |
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| Affiliation: | BAI Yuhong, ZHENG Qingping, HU Kefei (1.Yingkou Institure for Drug Control,Yingkou 115001 ,China;2.Beijing Institute of Increase Biology,Beijing 102209, China ) |
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| Abstract: | Objective:To establish a HPLC method to determine simultaneous assay in Zhenhuang Tablets. Methods: Ginsenoside Rg1, Ginsenoside Rb1and Notoginsenoside R1 were qualitatively measured by HPLC. Results: The linear relationship was respectively in the range from 1.144 to 11.440 μg for Ginsenoside Rg1, 0.948 to 9.480 μg for Ginsenoside Rb1, and 0.434 to 4.340 μg for Notoginsenoside R1 And the average recovery was 96.46%, 98.17% and 96.27%. Con-clusion: The method is efficient accurate and highly reproducible for the simultaneous assay of Zhenhuang tablets. |
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| Keywords: | Zhenhuang Tablets Simultaneous assay HPLC |
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