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安康口服液的制备及质量控制
引用本文:杜彪,刘友玲,何世新,陆星.安康口服液的制备及质量控制[J].中国药房,2005,16(19):1471-1472.
作者姓名:杜彪  刘友玲  何世新  陆星
作者单位:重庆市三峡精神卫生中心 重庆市404000 (杜彪,刘友玲),重庆市万州区药品检验所 重庆市404000 (何世新),重庆市万州区药品检验所 重庆市404000(陆星)
摘    要:目的:制备安康口服液并建立其含量测定方法。方法:用薄层色谱法对方中主药佛手、郁金进行定性鉴别,采用高效液相色谱法测定橙皮苷含量。结果:薄层色谱斑点清晰、集中,橙皮苷检测线性范围为0.04168μg~0.4168μg,平均回收率为98.11%,RSD=0.25%。结论:该制剂制备工艺简单,性质稳定,质量控制方法可行。

关 键 词:安康口服液  制备  质量控制  高效液相色谱法
文章编号:1001-0408(2005)19-1471-02
收稿时间:2005-04-27
修稿时间:2005-06-01

Preparation and Quality Control of Ankang Oral Liquid
Du Biao;Liu YouLing;He ShiXin;Liu Xing.Preparation and Quality Control of Ankang Oral Liquid[J].China Pharmacy,2005,16(19):1471-1472.
Authors:Du Biao;Liu YouLing;He ShiXin;Liu Xing
Abstract:OBJECTIVE:To prepare Ankang oral liquid and to establish its quality control method.METHODS:Qualiˉtation identification of the principal agents like Fructus citri sarcodactylis and Radix Curcumae were performed by TLC,the content of hesperidin was detemined by HPLC.RESULTS:The TLC spots were clear and centralized,the linear range of hesperidin was0.04168μg~0.4168μg,the average recovery was98.11%,RSD=0.25%.CONCLUSION:The preparing technique was simple and its quality is stable,the quality control method is accurate and feasible.
Keywords:Ankang oral liquid  Preparation  Quality control  HPLC
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