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青天葵乙酸乙酯部位化学成分的研究
引用本文:甄汉深,周燕园,袁叶飞,莫缓恒,钟振国,梁臣艳. 青天葵乙酸乙酯部位化学成分的研究[J]. 中药材, 2007, 30(8): 942-945
作者姓名:甄汉深  周燕园  袁叶飞  莫缓恒  钟振国  梁臣艳
作者单位:广西中医学院,广西南宁,530001
基金项目:国家自然科学基金;人事部留学回国人员科技活动择优基金;广西人事厅科研项目;广西高校人才小高地建设创新团队资助计划
摘    要:目的:对广西特产药材青天葵乙酸乙酯部位进行化学成分的研究。方法:采用硅胶柱层析,从青天葵乙酸乙酯部位中分离得到了5个化合物,并根据理化常数和光谱分析,对其进行结构鉴定。结果:5个单体化合物的结构分别为:正亮氨酸(norleucine,结晶Ⅰ)、24(S/β)-dihydrocycloeucalenol-(E)-p-hydroxy cinnamate(结晶Ⅱ)、鼠李柠檬素又名泻鼠李素(rhamnocitrin,结晶Ⅲ)、鼠李秦素又名甲基鼠李黄素(rhamnazin,结晶Ⅳ)、胡萝卜苷(dau-costerol,结晶Ⅴ)。结论:以上五种化合物首次从该植物中分离得到。

关 键 词:青天葵  化学成分
文章编号:1001-4454(2007)08-0942-04
修稿时间:2007-01-23

Studies on the Chemical Constituents of the Ethyl Acetate Portion of Nervilia fordii
ZHEN Han-shen,ZHOU Yan-yuan,YUAN Ye-fei,MO Huan-heng,ZHONG Zhen-guo,LIANG Chen-yan. Studies on the Chemical Constituents of the Ethyl Acetate Portion of Nervilia fordii[J]. Journal of Chinese medicinal materials, 2007, 30(8): 942-945
Authors:ZHEN Han-shen  ZHOU Yan-yuan  YUAN Ye-fei  MO Huan-heng  ZHONG Zhen-guo  LIANG Chen-yan
Affiliation:Guangxi University of Traditional Chinese Medicine, Nanning 530001 ,China
Abstract:OBJECTIVE: To study the chemical constituents of the ethyl acetate portion in the herb of Nervilia fordii from guangxi. METHODS: The constituents were separated and purified by using column chromatography with silica gel. These compounds were identified by their physical and spectral data. RESULTS: Five compounds were isolated and identified as norleucine (crystal I), 24 (S/beta)-dihydrocycloeucalenol-(E)-p-hydroxy cinnamate (crystal II) , rhamnocitrin (crystal III), rhamnazin (crystal IV), daucosterol (crystal V). CONCLUSION: Compounds I , II, III, IV, V were isolated from this plant for the first time.
Keywords:Nervilia fordii  Chemical constituents
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