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细叶桉叶超临界CO_2萃取挥发油的GC-MS分析
引用本文:周燕园,朱小勇,钟振国,贺海东.细叶桉叶超临界CO_2萃取挥发油的GC-MS分析[J].中国药房,2010(7):619-621.
作者姓名:周燕园  朱小勇  钟振国  贺海东
作者单位:广西中医学院,南宁市530001
基金项目:广西高校人才小高地建设创新团队资助计划项目
摘    要:目的:分析经超临界CO(2SFE-CO2)萃取的细叶桉叶挥发油的化学成分。方法:采用SFE-CO2法从细叶桉叶中提取挥发油,用气相色谱-质谱联用技术对其化学成分进行分析,并用归一化法确定各化学成分的相对百分含量。结果:细叶桉叶挥发油中共提取、鉴定出28种化合物,占色谱峰总面积的88.13%。其挥发性组分主要是桉油精(33.99%)、冰片(8.88%)、α-蒎烯(5.39%)、石竹烯(4.51%)、(+)-4-蒈烯(4.19%)等。结论:本研究可为细叶桉叶的进一步开发利用提供科学依据。

关 键 词:细叶桉  挥发油  超临界CO2萃取法  气相色谱-质谱联用技术

Component Analysis of Essential Oil Extracted with Supercritical CO2 from Eucalyptus tereticornis by GC-MS
ZHOU Yan-yuan,ZHU Xiao-yong,ZHONG Zhen-guo,HE Hai-dong.Component Analysis of Essential Oil Extracted with Supercritical CO2 from Eucalyptus tereticornis by GC-MS[J].China Pharmacy,2010(7):619-621.
Authors:ZHOU Yan-yuan  ZHU Xiao-yong  ZHONG Zhen-guo  HE Hai-dong
Institution:(Guangxi Traditional Chinese Medical University, Nanning 530001, China)
Abstract:OBJECTIVE:To analyze the chemical components extracted with supercritical CO2(SFE-CO2)from Eucalyptus tereticornis.METHODS: Volatile oil was extracted from E. tereticornis with SFE-CO2.The chemical component analyzed by GC-MS and its proportion was determined by normalization method. RESULTS: 28 compounds which account for 88.13% of the total peak area were separated and identified. The main components of volatile oil were eucalyptol (33.99%),borneol(8.88% ), α-pinene ( 5.39% ), caryophyllene (4.51% ), ( + )-4-carene (4.19%).CONCLUSION: This study can be served as a scientific basis for the further exploitation and utilization of E. tereticornis.
Keywords:Eucalyptus tereticornis  Essential oil  Supercritical CO2 extraction  GC-MS
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