| 固相微萃取GC-MS法分析大唇香科科、二齿香科科、长毛香科科的挥发油成分 |
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| 引用本文： | 陈青,张前军,杨占南,赵超,叶冲.固相微萃取GC-MS法分析大唇香科科、二齿香科科、长毛香科科的挥发油成分[J].中国药房,2010(11):1013-1016. |
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| 作者姓名： | 陈青 张前军 杨占南 赵超 叶冲 |
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| 作者单位： | [1]贵州大学理学院化学系,贵阳市550025 [2]贵州师范大学贵州省山地环境保护重点实验室,贵阳市550001 [3]贵州黄果树烟草集团技术中心,贵阳市550003 |
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| 基金项目： | 贵州省科学技术基金项目（黔科合J字[2006]2008号） |
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| 摘 要： | 目的:对大唇香科科、二齿香科科、长毛香科科的挥发油成分进行分析。方法:采用固相微萃取技术提取挥发油成分,用气相色谱-质谱联用技术对挥发油进行分析测定。结果:从大唇香科科、二齿香科科挥发油中共鉴定出33个化学成分,其中含量较高的组分为大栊牛儿烯-D(26.66%、27.88%)、1-辛烯-3-醇(13.19%、13.79%)、α-蒎烯(12.53%、13.07%)、β-芹子烯(5.93%、6.08%)、大栊牛儿烯-B(5.89%、6.20%)等。从长毛香科科挥发油中共鉴定出29个化学成分,其中含量较高的组分为石竹烯氧化物(21.52%)、α-甜没药萜醇(20.35%)、α-蒎烯氧化物(18.25%)、1-辛烯-3-醇(7.26%)、α-甜没药萜醇氧化物B(5.92%)等。结论:本试验可为香科科属植物资源的开发利用提供理论依据。
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| 关 键 词： | 大唇香科科 二齿香科科 长毛香科科 固相微萃取 气相色谱-质谱法 挥发油 成分 |
Component Analysis of Volatile Oil from Teuerium labiosum,T, bidentatant and T. pilosum by SPME/GC-MS |
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| CHEN Qing,ZHANG Qian-Jun,YANG Zhan-nan,ZHAO Chao,YE Chong.Component Analysis of Volatile Oil from Teuerium labiosum,T, bidentatant and T. pilosum by SPME/GC-MS[J].China Pharmacy,2010(11):1013-1016. |
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| Authors: | CHEN Qing ZHANG Qian-Jun YANG Zhan-nan ZHAO Chao YE Chong |
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| Institution: | (Dept. of Chemistry, School of Science of Guizhou University, Guiyang 550025, China ;Guizhou Provincial Key Laboratory for Mountainous Environment Protection, Guizhou Normal University, Guiyang 550001, China ;Technology Center of Guizhou Huangguoshu Tobacco Group, Guiyang 550003, China) |
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| Abstract: | OBJECTIVE： To analyze volatile oil from Teuerium labiosum, T. bidentatant and T. pilosum. METHODS ： Volatile oils were extracted from T. labiosum, T. bidentatant and T. pilosum using solid phase microextraction （SPME）. GC-MS was adopted to determine volatile oil. RESULTS ： 33 kinds of chemical components were identified in volatile oil of T. bidentatant and T. labiosum. The top 5 chemical components in list of content were Germacrene-D（26.66% and 27.88% ）, 1-octen-3-ol （13.19% and 13.79% ）, α-pinene（12.53% and 13.07% ）, β-selinene （5.93% and 6.08% ） and Germacrene-B （5.89% and 6.20% ）.29 chemical components were identified in volatile oil of T. lusitanicum with Caryophyllene oxide （21.52%） , α-bisabolol （20.35%） , α-pinene oxide （18.25%）, 1-octen-3-ol （7.26%）, and α-bisabolol oxide B （5.92%） as main constituents. CONCLUSION： The study provide theory basis for exploration of Teuerium. |
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| Keywords: | Teucrium labiosum Teucrium bidentatant Teucrium pilosum Solid phase microextraction GC-MS Volatile oil Component |
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