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妇炎散的质量标准研究
引用本文:李惠珍,苏松柏.妇炎散的质量标准研究[J].中国民族民间医药杂志,2012,21(15):50-51,57.
作者姓名:李惠珍  苏松柏
作者单位:贵阳中医学院第一附属医院,贵州贵阳,550001
基金项目:贵阳中医学院院内课题贵中医科院内[2010]29号:医院制剂“妇炎散”质量标准提升研究
摘    要:目的:建立妇炎散的质量标准.方法:采用薄层色谱法鉴别黄柏、姜黄、苍术等药材,采用高效液相色谱法测定妇炎散中盐酸小檗碱的含量.结果:该方法薄层色谱斑点清晰,阴性对照无干扰,盐酸小檗碱进样量在0.1015~1.015μg范围内呈良好线性关系(r=0.9999),平均加样回收率为97.97%.结论:所建标准可用于妇炎散的质量控制.

关 键 词:妇炎散  质量标准

Study of Quality Standards of Fu Yah San
LI Hui-zhen , SU Song-bai.Study of Quality Standards of Fu Yah San[J].Chinese Journal of Ethnomedicine and Ethnopharmacy,2012,21(15):50-51,57.
Authors:LI Hui-zhen  SU Song-bai
Institution:LI Hui - zhen SU Song - bai The First Affiliated Hospital of GuiYang college of Traditional Chinese Medicine, Guiyang 550001, China
Abstract:Objective: To establish the quality standard of Fu Yan San. Methods: The thin layer chromatography (TLC) was used to identify Cork, Turmeric, Atractylodes herbs, determine the content of of berberine hydrochloride in Fu Yan San By high per- formance liquid chromatography method (HPLC). Results: the methods TLC spots is clear and the negative control without interfer- ence, Berberine hydrochloride injection volume in the range of0. 1015 - 1. 015μg was good linear relationship (r =0. 9999) , aver- age recovery was 97.97%. Conclusion : Established standards can be used for quality control of Fu Yan San.
Keywords:Fu Yan San  Quality standard  Berberine Hydrochloride  Turmeric  Atractylodes
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