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热分析(TG,DTA)方法在鉴别贝母类中药材中的应用
引用本文:王书军,高文远,陈海霞,于璟琳,肖培根. 热分析(TG,DTA)方法在鉴别贝母类中药材中的应用[J]. 中国中药杂志, 2007, 32(4): 296-299
作者姓名:王书军  高文远  陈海霞  于璟琳  肖培根
作者单位:1. 天津大学,药物科学与生命技术学院,天津,300072
2. 天津大学,理学院,化学系,天津,300072
3. 中国医学科学院,中国协和医科大学,药用植物研究所,北京,100094
基金项目:科技部科技基础条件平台建设计划
摘    要:目的:提供一种快速简单的方法鉴别贝母类中药材。方法:采用热分析方法(TG,DTA)对9种贝母类中药材的热重/差热图谱进行分析。结果:通过分析9种不同贝母中药材粉末的热重/差热图谱发现,由于来源不同,地理环境和气候的差异,不同贝母类中药材的热分析图谱之间存在较大的差异。湖北贝母的热稳定性最高,平贝母的热稳定性最差,不同的贝母具有各自的差热图谱。结论:根据9种贝母中药材热分析图谱之间的差异,可以很容易的对其进行区分和鉴别。

关 键 词:贝母  热重/差热分析  鉴别
文章编号:1001-5302(2007)04-0296-04
收稿时间:2005-08-23
修稿时间:2005-08-23

Identification of Chinese medicine material of Fritillaria by themogravimetric/diffrential thermal analysis
WANG Shu-jun; GAO Wen-yuan; CHEN Hai-xia; YU Jing-lin; XIAO Pei-gen. Identification of Chinese medicine material of Fritillaria by themogravimetric/diffrential thermal analysis[J]. China Journal of Chinese Materia Medica, 2007, 32(4): 296-299
Authors:WANG Shu-jun   GAO Wen-yuan   CHEN Hai-xia   YU Jing-lin   XIAO Pei-gen
Affiliation:1. The College of Pharmaceutical Science and Biotechnology, Tianjin University, Tianjin 300072, China; 2. School of Science, Tianjin University, Tianfin 300072, China; 3. Institute of Medicinal Plant, Chinese Academy of Medical Sciences and Peking Union Medical College, Beifing 100094, China
Abstract:Objective: To provide a quick and simple method to identify different Chinese medicine material of Fritillaria. Method: The thermograms and differential thermograms of nine Fritillaria powders were obtained by thermal analyzer. Result: By analyzing the thermograms of nine Fritillaria powders, we concluded that the thermal stability of nine Fritillaria powders was much different each other due to the different geography origin. The thermal stability of F. hupehensis was highest among nine Fritillaria, while F. ussurensis was the lowest. The different Fritillaria showed their own DTA spectra respectively. Conclusion: According to the differences in the thermal properties of nine Fritillaria powders,the origins of Fritillaria could be easily identfied.
Keywords:Fritillaria   themogravimetric/ differential thermal analysis   identification
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