| 干柱层析法制备性分离冰片中龙脑和异龙脑 |
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| 引用本文： | 伍朝筼,杨胜华,吴苏澄. 干柱层析法制备性分离冰片中龙脑和异龙脑[J]. 四川大学学报(医学版), 1989, 0(3) |
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| 作者姓名： | 伍朝筼 杨胜华 吴苏澄 |
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| 作者单位： | 华西医大药学院药物分析研究室，华西医大药学院分析化学教研室，华西医大药学院 1988届毕业生 |
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| 摘 要： | 用干柱层析法,以硅胶为吸附剂,石油醚-醋酸乙酯-氯仿(20:2:6)为展开剂,在50×4cmi.d.柱上,下行展开,按龙脑和异龙脑在薄层板上的Rf值,初步判断柱上谱带的相应位置,分段切割,采用“打孔进样法”于薄层板上直接进样检试,分别收集龙脑和异龙脑谱带段吸附剂,用无水乙醇洗脱,减压回收溶剂,残液于冰箱中放置,即可得龙脑和异龙脑纯品。
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| 关 键 词： | 龙脑 异龙脑 干柱层析法 |
PREPARATIVE SEPARATION OF BORNEOL AND ISOBORNEOL IN BINGPIAN BY DRYCOLUMN CHROMATOGRAPHY |
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| Wu Chaoyuan,Yang Shenghua,Wu Sucheng Laboratory of Pharmaceutic Analysis. PREPARATIVE SEPARATION OF BORNEOL AND ISOBORNEOL IN BINGPIAN BY DRYCOLUMN CHROMATOGRAPHY[J]. Journal of Sichuan University. Medical science edition, 1989, 0(3) |
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| Authors: | Wu Chaoyuan Yang Shenghua Wu Sucheng Laboratory of Pharmaceutic Analysis |
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| Affiliation: | Wu Chaoyuan,Yang Shenghua,Wu Sucheng Laboratory of Pharmaceutic Analysis,Department of Analytical Chemistry,School of Pharmacy |
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| Abstract: | |
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| Keywords: | Borneol Isoborneol Dry-column chromatography |
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