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| 达斯玛保丸质量标准研究 | |
| 引用本文： | 李玲莉,王兰霞,倪琳,杨锡,张妍,张晓萍,田喜莲.达斯玛保丸质量标准研究[J].中国中医药信息杂志,2011,18(10):62-64. |
| 作者姓名： | 李玲莉 王兰霞 倪琳 杨锡 张妍 张晓萍 田喜莲 |
| 作者单位： | 1. 甘肃中医学院,甘肃兰州,730000 2. 甘肃省食品药品检验所,甘肃兰州,730000 3. 兰州大学药学院,甘肃兰州,730000 4. 甘肃奇正藏药有限公司,甘肃兰州,730000 |
| 摘 要： | 目的建立达斯玛保丸的质量标准。方法采用薄层色谱法对处方中木香、紫草茸、翼首草、藏茜草、安息香进行定性鉴别;采用高效液相色谱法测定诃子中没食子酸的含量。结果薄层色谱鉴别方法专属性强,阴性无干扰;没食子酸在0.485～4.850μg内呈良好线性关系（r=0.999 3）,平均回收率为99.31%,RSD=1.12%（n=9）。结论本方法准确、简便、专属性强、重复性好,可用于达斯玛保丸的质量控制。 |
| 关 键 词： | 达斯玛保丸 薄层色谱法 高效液相色谱法 没食子酸 质量标准 |
Study on Quality Standard for Dasimabao Pills |
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| LI Ling-li,WANG Lan-xia,NI Lin,YANG Xi,ZHANG Yan,ZHANG Xiao-ping,TIAN Xi-lian.Study on Quality Standard for Dasimabao Pills[J].Chinese Journal of Information on Traditional Chinese Medicine,2011,18(10):62-64. | |
| Authors: | LI Ling-li WANG Lan-xia NI Lin YANG Xi ZHANG Yan ZHANG Xiao-ping TIAN Xi-lian |
| Institution: | LI Ling-li1,WANG Lan-xia2,NI Lin2,YANG Xi2,ZHANG Yan3,ZHANG Xiao-ping3,TIAN Xi-lian4(1.Gansu College of TCM,Lanzhou 730000,China,2.Gansu Institute for Food and Drug Control,3.School of Pharmacy,Lanzhou University,4.Gansu Cheezheng Tibetan Medicine Co.,Ltd,China) |
| Abstract: | Objective To establish the quality standard of Dasimabao Pills.Methods Radix Aucklandiae,Lac Lacca,Hooker winghead root,Radix Et Rhizoma Rubiae and Benzoin were identified by TLC.The content of gallic acid in Dasimabao Pills was determined by HPLC.Results The characteristic of identification by TLC was distinct and highly specific.The linear range of gallic acid was 0.485-4.850 μg（r=0.999 3）.The average recovery was 99.31% and RSD was 1.12%（n=9）.Conclusion The method is accurate and convinient,with good specifity and reproducibility,and can be used for the quality control of Dasimabao Pills. |
| Keywords: | Dasimabao Pills TLC HPLC gallic acid quality standard |
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