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四角蛤蜊软体中脂肪酸成分的GC-MS分析
引用本文:程建明,嵇晶,刘睿,王令充,吴皓.四角蛤蜊软体中脂肪酸成分的GC-MS分析[J].中国实验方剂学杂志,2013,19(19):114-117.
作者姓名:程建明  嵇晶  刘睿  王令充  吴皓
作者单位:南京中医药大学药学院, 南京 210046;江苏省海洋药物研究开发中心, 南京 210029;南京中医药大学药学院, 南京 210046;江苏省海洋药物研究开发中心, 南京 210029;南京中医药大学药学院, 南京 210046;江苏省海洋药物研究开发中心, 南京 210029;南京中医药大学药学院, 南京 210046;江苏省海洋药物研究开发中心, 南京 210029;南京中医药大学药学院, 南京 210046;江苏省海洋药物研究开发中心, 南京 210029
基金项目:国家自然科学基金项目(30900293);南京中医药大学青年自然科学基金项目(11XZR10);南京中医药大学科技创新风险基金项目(CX201105)
摘    要:目的: 分析四角蛤蜊软体中脂肪酸类成分。方法: 以Bligh-Dyer法萃取四角蛤蜊软体中脂肪酸,经甲酯化后利用气相色谱-质谱联用技术对其脂肪酸组成进行了分析和鉴定。结果: 共分离鉴定出22种脂肪酸,占总脂肪酸含量的82.51%。其中饱和脂肪酸的相对含量为24.35%,主要为十八酸、十六烷酸;不饱和脂肪酸的相对含量为58.16%,主要为9-十六烯酸、11-二十烯酸、十四烯酸及5,8,11,14-二十碳四烯酸。结论: 四角蛤蜊软体中含有丰富的脂肪酸芙物质,具有较好的开发价值。

关 键 词:四角蛤蜊  脂肪酸  气相色谱法-质谱联用
收稿时间:2012/5/11 0:00:00

GC-MS Analysis of Fatty Acid from Mactra veneriformis
CHEN Jian-ming,JI Jing,LIU Rui,WANG Ling-chong and WU Hao.GC-MS Analysis of Fatty Acid from Mactra veneriformis[J].China Journal of Experimental Traditional Medical Formulae,2013,19(19):114-117.
Authors:CHEN Jian-ming  JI Jing  LIU Rui  WANG Ling-chong and WU Hao
Institution:College of Pharmaceutical Science, Nanjing University of Chinese Medicine, Nanjing 210046, China;Research Center of Marine Drug in Jiangsu Province, Nanjing 210029, China;College of Pharmaceutical Science, Nanjing University of Chinese Medicine, Nanjing 210046, China;Research Center of Marine Drug in Jiangsu Province, Nanjing 210029, China;College of Pharmaceutical Science, Nanjing University of Chinese Medicine, Nanjing 210046, China;Research Center of Marine Drug in Jiangsu Province, Nanjing 210029, China;College of Pharmaceutical Science, Nanjing University of Chinese Medicine, Nanjing 210046, China;Research Center of Marine Drug in Jiangsu Province, Nanjing 210029, China;College of Pharmaceutical Science, Nanjing University of Chinese Medicine, Nanjing 210046, China;Research Center of Marine Drug in Jiangsu Province, Nanjing 210029, China
Abstract:Objective: The purpose of this study was to analyze the fatty acid from Mactra veneriformis. Method: The fatty acid in flesh was extracted by the method of Bligh-Dyer. Fatty acid was methyl esterified and then analyzed by gas chromatography-mass spectrometry. Result: Twenty\|two components were identified, representing 82.51% of the total constituents, in which the saturated fatty acid represent 24.35% and the unsaturated fatty acid represent 58.16%. The major components in saturated fatty acid were octadecanoic acid and hexadecanoic acid, the major components in unsaturated fatty acid were 9,12-hexadecanoic acid, 11-eicosenoic acid, tetradecenoic acid and 5,8,11,14-eicosatetraenoic acid. Conclusion: M. Veneriformis is rich in facty acid and can be developed in the future.
Keywords:Mactra veneriformis  fatty acid  GC-MS
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