| 癌痛平胶囊质量控制研究 |
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| 引用本文： | 张裕强,朱华旭,郭立玮. 癌痛平胶囊质量控制研究[J]. 现代中药研究与实践, 2008, 22(1): 41-43 |
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| 作者姓名： | 张裕强 朱华旭 郭立玮 |
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| 作者单位： | 南京中医药大学中医药研究院,江苏,南京,210029 |
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| 基金项目： | 江苏省天然药物研究与创制实验室开放课题(编号:KF2005001) |
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| 摘 要： | 目的建立癌痛平胶囊的质量标准。方法采用薄层色谱鉴别癌痛平胶囊中蚤休（重楼）、制乳香药材及用高效液相色谱法测定胡椒碱的含量。结果TLC能检出蚤休和制乳香，且阴性对照无干扰；胡椒碱在6．2968～201．5μg·mL^-1之间呈良好的线性关系，相关系数r=1．0000，平均加样回收率为99．24％，RSD=2．25％。结论该法操作简便、结果准确、重现性好，适用于癌痛平胶囊的质量标准研究。
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| 关 键 词： | 癌痛平胶囊 薄层色谱法 高效液相色谱法 胡椒碱 |
| 文章编号： | 1673-6427(2008)01-0041-03 |
| 修稿时间： | 2007-08-19 |
Study on the Quality Standards of Aitongping Capsules |
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| ZHANG Yu-qiang,ZHU Hua-xu,GUO Li-wei. Study on the Quality Standards of Aitongping Capsules[J]. Research and Practice on Chinese Medicines, 2008, 22(1): 41-43 |
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| Authors: | ZHANG Yu-qiang ZHU Hua-xu GUO Li-wei |
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| Affiliation: | ( Institute of TCM, Nanjing University of Traditional Chinese Medicine, Nanjing 210029, China) |
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| Abstract: | Objective To establish the quality standards of Aitongping capsules.Methods TLC methods for identification of Rhizoma Paridis and Concocting Frankincense were established.A HPLC method was established for the determination of piperine.Results The spots on TLC plates were clear without interference in the blank reference.The liner range of piperine was 6.2968～201.5μg· mL-1,r=1.000 0.The average recovery of piperine was 99.24% and RSD=2.25%.Conclusion The method is simple,accurate,reproducible and can be used for the quality standards of Aitongping capsules. |
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| Keywords: | Aitongping capsules TLC HPLC piperine |
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