| 微米红参的制备及含量测定 |
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| 引用本文： | 杨凯,石莹,李镐,郭建鹏.微米红参的制备及含量测定[J].中国实验方剂学杂志,2010,16(14):17-19. |
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| 作者姓名： | 杨凯 石莹 李镐 郭建鹏 |
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| 作者单位： | 1. 延边大学药学院,吉林,延吉,133000
2. 延边大学药学院,吉林,延吉,133000;长白山生物资源与功能分子教育部重点实验室,吉林,延吉,133002 |
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| 基金项目： | 吉林省科技发展计划项目，吉林省教育厅"十一五"科学技术研究项目 |
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| 摘 要： | 目的:优化微米红参的制备工艺,测定其主要人参皂苷含量。方法:采用单因素法对影响红参微米化因素进行筛选,以平均粒径和粒度分布为考察指标,优化微米红参化生产的最佳工艺;采用高效液相色谱法测定人参皂苷Rg1,Re,Rb1的含量。结果:最佳工艺为风袋长度20 cm,粉碎时间为40 min,单次进料量为500 g;测得样品中人参皂苷Rg1,Re,Rb1的含量分别2.06,1.77,2.41 mg.g-1,微米红参人参皂苷含量测定显著高于红参普通粉与切片。结论:微米红参制备工艺合理、稳定;建立的含量测定方法适用于微米红参;微米红参利于人参皂苷成分溶出。
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| 关 键 词： | 超微粉碎 人参皂苷 高效液相 |
| 收稿时间： | 2010/6/12 0:00:00 |
Preparation and Content Determination of Micron Red Ginseng |
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| YANG Kai,SHI Ying,LI Gao and GUO Jian-peng.Preparation and Content Determination of Micron Red Ginseng[J].China Journal of Experimental Traditional Medical Formulae,2010,16(14):17-19. |
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| Authors: | YANG Kai SHI Ying LI Gao and GUO Jian-peng |
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| Institution: | YANG Kai1,SHI Ying,LI Gao1,GUO Jian-peng1,2(1.College of Pharmacy,Yanbian University,Yanji 133000,China,2.Key Laboratory of Natural Resources of Changbai Mountain & Functional Molecules,Ministry of Education,Yanji 133002,China) |
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| Abstract: | Objective:The preparation process optimization of microns red Ginseng was performed with de-tection of ginsenoside.Method:The single factor law on the factors affected red Ginseng microns in diameter screening,particle size distribution to optimize the production of red Ginseng microns optimum technology.The gin-senoside Rg1,Re and Rb1 were determined by HPLC.Result:The best process was as follows:the wind bag length was 20 cm,crushing time 40 min into the charge for a single 500 g;the concent of ginsenosid... |
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| Keywords: | ultra-fine pulverizing ginsenoside HPLC |
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