| 顶空进样GC-MS结合保留指数分析补骨脂挥发性成分 |
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| 引用本文： | 刘朋,徐琳琳,吕青涛,巩丽丽,容蓉.顶空进样GC-MS结合保留指数分析补骨脂挥发性成分[J].中国实验方剂学杂志,2011,17(10):74-76. |
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| 作者姓名： | 刘朋 徐琳琳 吕青涛 巩丽丽 容蓉 |
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| 作者单位： | 1. 山东中医药大学,济南,250355
2. 山东齐都药业有限公司,山东淄博,255400 |
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| 基金项目： | 国家重点基础研究发展计划("973"计划)(2007CB512601)项目 |
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| 摘 要： | 目的:分析补骨脂中的挥发性成分。方法:采用顶空直接进样技术采集补骨脂的挥发性成分,GC-MS结合保留指数进行分析鉴定。结果:采用GC-MS分析,检出39个组分;MS结合保留指数定性,鉴定出20个挥发性成分。结论:该方法分析补骨脂中挥发性成分,更准确、简单、快速并节省药材。
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| 关 键 词： | 补骨脂 挥发性成分 气相色谱质谱仪 保留指数 顶空进样 |
| 收稿时间： | 2010/11/29 0:00:00 |
GC-MS Combined with Kovats Retention Index Analysis for Volatile Compounds in Psoraleae Fructus by Headspace Injection |
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| LIU Peng,XU Lin-lin,LV Qing-tao,GONG Li-li and RONG Rong.GC-MS Combined with Kovats Retention Index Analysis for Volatile Compounds in Psoraleae Fructus by Headspace Injection[J].China Journal of Experimental Traditional Medical Formulae,2011,17(10):74-76. |
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| Authors: | LIU Peng XU Lin-lin LV Qing-tao GONG Li-li and RONG Rong |
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| Institution: | College of Pharmacy, Shandong University of Traditional Chinese Medicine, Jinan 250355, China;Shandong Qidu Pharmaceutical Co., Ltd. Zibo 255400, China;College of Pharmacy, Shandong University of Traditional Chinese Medicine, Jinan 250355, China;College of Pharmacy, Shandong University of Traditional Chinese Medicine, Jinan 250355, China;College of Pharmacy, Shandong University of Traditional Chinese Medicine, Jinan 250355, China |
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| Abstract: | Objective: To analyze the volatile compounds in Psoraleae Fructus. Method :Volatile components in Psoraleae Fructus were analyzed and identified by GC-MS combined with Kovats retention index by head-space injection. Result: Thirty-nine components in Psoraleae Fructus were detected by GC-MS and 20 compounds were identified by MS combined with Kovats retention index. Conclusion: GC-MS combined with Kovats retention index by headspace injection is a simple,rapid and accurate way for the analysis of volatile compounds in Psoraleae Fructus. |
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| Keywords: | Psoraleae Fructus volatile compounds GC-MS Kovats retention index headspace injection |
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