| HPLC同时测定五味子中6种木脂素类成分 |
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| 引用本文： | 黄文倩,李丽,肖永庆,张村,于定荣,麻印莲,田国芳,王云.HPLC同时测定五味子中6种木脂素类成分[J].中国实验方剂学杂志,2011,17(10):63-66. |
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| 作者姓名： | 黄文倩 李丽 肖永庆 张村 于定荣 麻印莲 田国芳 王云 |
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| 作者单位： | 1. 首都医科大学中医药学院,北京,100069;中国中医科学院中药研究所,北京,100700
2. 首都医科大学中医药学院,北京,100069 |
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| 摘 要： | 目的:建立同时测定五味子中6种木脂素类成分的HPLC含量测定方法。方法:采用HPLC,以甲醇-0.5%冰醋酸为流动相,梯度洗脱,检测波长254 nm,流速0.9 mL.min-1,柱温35℃,同时测定五味子药材中五味子甲素、五味子乙素、五味子丙素、五味子醇甲、五味子醇乙、五味子酯甲等6种木脂素类成分的含量。结果:不同产地五味子药材中均含有上述6种成分,且均以五味子醇甲的含量最高,五味子丙素含量最低。结论:建立的方法可以同时测定五味子药材中的6种木脂素类成分,为五味子及其炮制品的质量评价提供了更为全面的科学依据。
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| 关 键 词： | 五味子 木脂素 含量测定 |
| 收稿时间： | 2010/12/29 0:00:00 |
Simultaneous Determination of Six Lignan Components in Schisandrae Chinensis Fructus by HPLC |
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| HUANG Wen-qian,LI Li,XIAO Yong-qing,ZHANG Cun,YU Ding-rong,MA Yin-lian,TIAN Guo-fang and WANG Yun.Simultaneous Determination of Six Lignan Components in Schisandrae Chinensis Fructus by HPLC[J].China Journal of Experimental Traditional Medical Formulae,2011,17(10):63-66. |
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| Authors: | HUANG Wen-qian LI Li XIAO Yong-qing ZHANG Cun YU Ding-rong MA Yin-lian TIAN Guo-fang and WANG Yun |
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| Institution: | 1.College of Traditional Chinese Medicine, Capital Medical Univercity, Beijing 100069, China; 2.Institute of Chinese Mateia Madica, China Academy of Chinese Medical Sciences, Beijing 100700, China;1.College of Traditional Chinese Medicine, Capital Medical Univercity, Beijing 100069, China; 2.Institute of Chinese Mateia Madica, China Academy of Chinese Medical Sciences, Beijing 100700, China;1.College of Traditional Chinese Medicine, Capital Medical Univercity, Beijing 100069, China; 2.Institute of Chinese Mateia Madica, China Academy of Chinese Medical Sciences, Beijing 100700, China;1.College of Traditional Chinese Medicine, Capital Medical Univercity, Beijing 100069, China; 2.Institute of Chinese Mateia Madica, China Academy of Chinese Medical Sciences, Beijing 100700, China;1.College of Traditional Chinese Medicine, Capital Medical Univercity, Beijing 100069, China; 2.Institute of Chinese Mateia Madica, China Academy of Chinese Medical Sciences, Beijing 100700, China;1.College of Traditional Chinese Medicine, Capital Medical Univercity, Beijing 100069, China; 2.Institute of Chinese Mateia Madica, China Academy of Chinese Medical Sciences, Beijing 100700, China;1.College of Traditional Chinese Medicine, Capital Medical Univercity, Beijing 100069, China; 2.Institute of Chinese Mateia Madica, China Academy of Chinese Medical Sciences, Beijing 100700, China;1.College of Traditional Chinese Medicine, Capital Medical Univercity, Beijing 100069, China; 2.Institute of Chinese Mateia Madica, China Academy of Chinese Medical Sciences, Beijing 100700, China |
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| Abstract: | |
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| Keywords: | Schisandrae Chinensis Fructus lignan content determination |
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