| 祛瘀生新胶囊挥发性部位研究 |
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| 引用本文： | 郭冬,王洪波,杜霞,张红,李彤晖. 祛瘀生新胶囊挥发性部位研究[J]. 西北药学杂志, 2016, 0(6): 568-571. DOI: 10.3969/j.issn.1004-2407.2016.06.005 |
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| 作者姓名： | 郭冬 王洪波 杜霞 张红 李彤晖 |
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| 作者单位： | 陕西省中医药研究院,西安,710003 |
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| 基金项目： | 陕西省科学技术研究发展计划项目(2011k12-03-05) |
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| 摘 要： | 目的筛选祛瘀生新胶囊挥发油部位提取工艺并建立质量标准。方法以L9(34)正交实验,考察挥发油提取及包合条件,以HPLC定量及TLC定性控制挥发油包合物质量。结果提取工艺为:加9倍量水,浸泡1h,提取9h;包合工艺为:挥发油∶β-环糊精=1∶11,包合时间3h,包合温度40℃;建立了挥发油包合物质量标准。结论优化后工艺可操作性强、稳定、合理,质量控制标准专一、全面、可行。
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| 关 键 词： | 祛瘀生新胶囊 挥发性部位 正交实验 质量标准 |
Research of the volatile part for Quyushengxin Capsules |
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| Abstract: | Objective To screen the extract procedure and establish the quality standard of the volatile oil for Quyushengxin Cap-sules.Methods The orthogonal test L9 (3 4 )was used to investigate the degree of extraction and inclusion for the volatile oil.The quality of the inclusion compound for the volatile was controlled by HPLC and TLC.Results The extraction procedure:9 times water,soak for 1 h,extraction 9 h.The inclusion procedure,volatile oil∶ β-cyclodextrin= 1 ∶ 1 1,inclusion time 3 h,and the package junction temperature 40 ℃.Conclusion The optimized process is feasible,stable and reasonable.The quality control standard is specific,comprehensive and feasible. |
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| Keywords: | Quyushengxin Capsules volatile site orthogonal test quality standard |
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