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| 萝卜秦艽化学成分的研究Ⅱ | |
| 引用本文： | 余振喜,王钢力,戴忠,边巴次仁,林瑞超.萝卜秦艽化学成分的研究Ⅱ[J].中国药学杂志,2007,42(17):1295-1298. |
| 作者姓名： | 余振喜 王钢力 戴忠 边巴次仁 林瑞超 |
| 作者单位： | 1. 北京中医药大学中药学院,北京,100102;中国药品生物制品检定所,北京,100050 2. 中国药品生物制品检定所,北京,100050 3. 西藏自治区药品检验所,拉萨,850000 |
| 摘 要： | 目的对萝卜秦艽的化学成分进行研究。方法采用大孔树脂、薄层色谱和硅胶柱色谱等方法进行分离纯化,通过理化方法和波谱数据进行结构鉴定。结果从体积分数95%乙醇提取物大孔树脂体积分数95%乙醇洗脱物中分离并鉴定了10个化合物,分别为phlomisoic acid(Ⅰ)、phlomisoside Ⅴ(Ⅱ)、phlomisosideⅢ(Ⅲ)、三十烷酸(Ⅳ)、三十烷酸对羟基苯乙酯(Ⅴ)、邻苯二甲酸正丁异丁酯(Ⅵ)、棕榈酸(Ⅶ)、油酸(Ⅷ)、β-谷甾醇(Ⅸ)和胡萝卜苷(Ⅹ)。结论除Ⅲ外,其余化合物均为首次从该植物中分得,其中Ⅳ、Ⅴ、Ⅵ为首次从该属植物中分得,Ⅱ为一新化合物。 |
| 关 键 词： | 萝卜秦艽 化学成分 phlomisosideⅤ |
| 文章编号： | 1001-2494（2007）17-1295-04 |
| 收稿时间： | 2006-03-08; |
| 修稿时间： | 2006-03-08 |
Studies on Chemical Constituents of Phlomis medicinalis Ⅱ |
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| YU Zhen-xi,WANG Gang-li,DAI Zhong,BIANBA Ci-ren,LIN Rui-chao.Studies on Chemical Constituents of Phlomis medicinalis Ⅱ[J].Chinese Pharmaceutical Journal,2007,42(17):1295-1298. | |
| Authors: | YU Zhen-xi WANG Gang-li DAI Zhong BIANBA Ci-ren LIN Rui-chao |
| Institution: | 1. College of Chinese Materia Medica, Belting University of Traditional Chinese Medicine, Beifing 100102, China; 2. National Institute for the Control of Pharmaceutical and Biological Products, Beijing 100050, China ; 3. Tibet Institute for Drug Control, Lhasa 850000, China |
| Abstract: | OBJECTIVE To study the chemical constituents of Phlomis medicinalis.METHODS The compounds were isolated and repeatedly purified on macroporous resin,silica gel column chromatograph and TLC and the structures were elucidated by physico-chemical properties and spectral analysis.RESULTS Ten compounds were obtained and elucidated as phlomisoic acid(Ⅰ),phlomisoside Ⅴ(Ⅱ),phlomisoside Ⅲ(Ⅲ),triacontanoic acid(Ⅳ),triacontanoic acid,2-(4-hydroxyphenyl)ethyl ester(Ⅴ),phthalic acid,butyl isobutyl ester(Ⅵ),palmitic acid(Ⅶ),oleic acid(Ⅷ),β-sitosterol(Ⅸ)and daucosterol(Ⅹ).CONCLUSION They have been isolated from this plant for the first time besides compound Ⅲ,and compound Ⅳ,Ⅴ and Ⅵ were obtained from the plants of Phlomis for the first time,and phlomisoside Ⅴ was a new compound. |
| Keywords: | Phlomis medicinalis chemical constituents phlomisoside V |
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