| 高效液相色谱法测定大米中残留的咪唑磺隆 |
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| 引用本文： | 张曼,何佳,古珑,林安清,许泓,张骏. 高效液相色谱法测定大米中残留的咪唑磺隆[J]. 口岸卫生控制, 2006, 11(6): 23-24 |
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| 作者姓名： | 张曼 何佳 古珑 林安清 许泓 张骏 |
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| 作者单位： | 天津出入境检验检疫局,天津,300201;天津出入境检验检疫局,天津,300201;天津出入境检验检疫局,天津,300201;天津出入境检验检疫局,天津,300201;天津出入境检验检疫局,天津,300201;天津出入境检验检疫局,天津,300201 |
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| 摘 要： | 目的本方法为大米中咪唑磺隆残留量的检测技术。方法样品提取后采用自动固相萃取方式;定量分析采用高效液相色谱方法-紫外检测器进行检测。结果最低检测限为0．02 mg／kg;大米中残留咪唑磺隆量实验精密度为2．23％-5．66％;咪唑磺隆的添加浓度在0．02 mg／kg-0．50 mg／kg时,回收率范围为88．5％-90．7％。结论该方法具有高效率,高灵敏度,准确度好,可靠性高等技术特点。
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| 关 键 词： | 高效液相色谱 大米 咪唑磺隆 |
| 收稿时间： | 2006-09-30 |
| 修稿时间： | 2006-09-30 |
Determination of imazosulfuron in cereals by HPLC |
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| Zhang Man,He Jia,Gu Long,Lin Anqing,Xu Hong,Zhang Jun. Determination of imazosulfuron in cereals by HPLC[J]. , 2006, 11(6): 23-24 |
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| Authors: | Zhang Man He Jia Gu Long Lin Anqing Xu Hong Zhang Jun |
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| Abstract: | Objective In this paper a method for determination of imazosulfuron in cereals by HPLC was described. Methods Samples were cleaned up with auto solid phase extraction and determined by HPLC using UV-detector. Results The detection limits were 0.02 mg/kg, recoveries and RSDs of the method were 88.5%- 90.7% and 2.23%-5.66% at this concentration. Conclusion The method described has high efficiency and sensitivity, with good stability and veracity. |
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| Keywords: | HPLC Cereal Imazosulfuron |
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