高效液相色谱法测定肌氨肽苷注射液中次黄嘌呤的含量 |
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引用本文: | 李明兰,秦香芹.高效液相色谱法测定肌氨肽苷注射液中次黄嘌呤的含量[J].黑龙江医药,2012,25(2):192-193. |
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作者姓名: | 李明兰 秦香芹 |
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作者单位: | 1. 哈尔滨圣泰制药股份有限公司 2. 哈尔滨瀚邦医疗科技有限公司 |
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摘 要: | 目的:建立高效液相色谱法测定肌氨肽苷注射液中次黄嘌呤的含量。方法:以十八烷基硅烷键合硅胶为填充剂,磷酸二氢钾(0.01mol/L)-甲醇(100:0.2)为流动相,检测波长260nm。结果:平均回收率为100.56%,RSD=1.57%。结论:该方法简便、准确。
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关 键 词: | 高效液相色谱法 肌氨肽苷注射液 次黄嘌呤 |
Determination of Hypoxanthine in Jiantaigan Injection by HPLC |
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Institution: | Li Minglan1,et al 1.Harbin Sanctity Pharmaceutical Co Ltd. |
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Abstract: | Objective:To establish a method of hypoxanthine for Jiantaigan injection by high-performance liquid chromatography.Methods:The method uses a C18 column,potassium dihydrogen phosphate(0.01mol/L)-methanol(100:0.2)as the mobile phase.The detection wavelength was set at 260nm.Results:The average recovery was 100.56%,RSD was 1.57%.Conclusion:The method is simple and accurate. |
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Keywords: | High-performance liquid chromatography Jiantaigan Injection Hypoxanthine |
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