| 反相高效液相色谱法测定消炎颗粒中黄芩苷的含量 |
| |
| 引用本文： | 秦红霖. 反相高效液相色谱法测定消炎颗粒中黄芩苷的含量[J]. 药学实践杂志, 2003, 21(4): 218-219 |
| |
| 作者姓名： | 秦红霖 |
| |
| 作者单位： | 北京军区药检所,北京,100071 |
| |
| 摘 要： | 目的：测定消炎颗粒中黄芩苷的含量。方法：RP-HPLC法，采用C18分析柱，甲醇-0．2％磷酸(60：40)为流动相，检测波长为280nm。结果：该法平均回收率为100．64％，RSD=1．69％(n=5)。结论：本法快速、准确，样品处理简便易行，重现性好。
|
| 关 键 词： | 消炎颗粒 黄芩苷 含量测定 反相高效液相色谱法 RP-HPLC法 C18分析柱 中药复方制剂 |
| 文章编号： | 1006-0111(2003)04-0218-02 |
| 收稿时间： | 2003-03-31 |
| 修稿时间： | 2003-03-31 |
Determination of baicalin in Xiaoyan granules by RP-HPLC |
| |
| QIN Hong-lin. Determination of baicalin in Xiaoyan granules by RP-HPLC[J]. The Journal of Pharmaceutical Practice, 2003, 21(4): 218-219 |
| |
| Authors: | QIN Hong-lin |
| |
| Affiliation: | Institute for Drug Control of Beijing Command of PLA, Beijing 100071, China |
| |
| Abstract: | OBJECTIVE: To determine the content of baicalin in Xiaoyan granules. METHODS: Re verse-phase high performance liquid chromatography was established. A C18 column (250mmX 4. 6mm,5um) with mobile phase of MeOH:0. 2%phosphat (60 : 40) was used. The detection wavelength was 280nm. RESULTS:The mean recoveries were 100.64% (RSD -1.69% ). CONCLUSION:The method was rapid, sensitive and accurate. |
| |
| Keywords: | RP-HPLC Xiaoyan granules baicalin |
| 本文献已被 CNKI 维普 万方数据 等数据库收录！ |
| 点击此处可从《药学实践杂志》浏览原始摘要信息 |
|
点击此处可从《药学实践杂志》下载全文 |
