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大孔吸附树脂富集藏药镰形棘豆总黄酮的工艺研究
引用本文:刘延彤,李茂星,杜青云,张汝学,贾正平.大孔吸附树脂富集藏药镰形棘豆总黄酮的工艺研究[J].药学实践杂志,2008,26(6):428-440.
作者姓名:刘延彤  李茂星  杜青云  张汝学  贾正平
作者单位:1. 兰州军区总医院药材科,甘肃,兰州,730050
2. 中国人民解放军第175医院药材科,福建,漳州,350005
基金项目:军队医药卫生科研项目 , 南京军区医约卫生科研课题  
摘    要:目的:建立镰形棘豆总黄酮的大孔吸附树脂富集工艺.方法:二氯氧锆比色法测定样品中总黄酮苷含量,考察D-101大孔吸附树脂富集镰形棘豆水提取物中总黄酮的动态吸附能力,解吸附溶媒浓度及体积,以及树脂的重复利用能力等.结果:富集后总黄酮苷含量达到26%,接近富集前的5倍.结论:D-101型大孔吸附树脂对镰形棘豆水提物中总黄酮成分有较好的吸附能力,60%乙醇溶液解吸附快速有效,树脂重复利用度高.

关 键 词:镰形棘豆  总黄酮  大孔吸附树脂  工艺
收稿时间:2008/3/24 0:00:00

Study on enriching technic process of total flavones from Herba Oxytropis Falcatae by macroporous resin
LIU Yan-tong,LI Mao-xing,DU Qing-yun,ZHANG Ru-xue and JIA Zheng-ping.Study on enriching technic process of total flavones from Herba Oxytropis Falcatae by macroporous resin[J].The Journal of Pharmaceutical Practice,2008,26(6):428-440.
Authors:LIU Yan-tong  LI Mao-xing  DU Qing-yun  ZHANG Ru-xue and JIA Zheng-ping
Institution:LIU Yan-tong~1 LI Mao-xing~1 DU Qing-yun~2 ZHANG Ru-xue~1 JIA Zheng-ping~1(1.Department of Pharmacy,Lanzhou General Hospital of PLA,Lanzhou 730050,China,2.Department of Pharmacy,the 175th Hospital of PLA,Zhangzhou 350005,China)
Abstract:Objective:To establish an enriching technic process of total flavones from Herba Oxytropis Falcatae by macroporous resin.Methods:Zirconium oxychloride(ZrOCl_2)chromatometry was used to determine the content of total flavones in samples.Dynamic state adsorbability,concentration and volume of adsorption stripping solvent,and the re-utilization of D-101 macroporous resin were studied.Results:The content of total flavones in enrichment is 26%,which was nearly five times of that before enriched.Conclusion: Chrom...
Keywords:Herba Oxytropis falcatae  total flavones  D-101 macroporous resin  enriching technic process  
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