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高效液相色谱法测定舒肝丸中芍药苷含量
引用本文:孙大鹏. 高效液相色谱法测定舒肝丸中芍药苷含量[J]. 现代中药研究与实践, 2006, 20(2): 32-33
作者姓名:孙大鹏
作者单位:哈药集团制药六厂,黑龙江,哈尔滨,150056
摘    要:目的建立舒肝丸中芍药苷含量测定方法。方法采用C18柱,以甲醇∶水(25∶75)为流动相,检测波长为243 nm。结果线性范围为0.20~1.00μg,本法回收率为99.88%,RSD为1.41%。结论本法操作简便易行,可供舒肝丸中芍药苷质量控制用。

关 键 词:舒肝丸  芍药苷  高效液相色谱法
文章编号:1004-2199(2006)02-0032-02
收稿时间:2005-01-20
修稿时间:2005-01-20

Determination of Paeoniflorin in Shugan Pills by HPLC
SHUN Da-peng. Determination of Paeoniflorin in Shugan Pills by HPLC[J]. Research and Practice on Chinese Medicines, 2006, 20(2): 32-33
Authors:SHUN Da-peng
Affiliation:The Sixth Pharmaceutical Factory, Harbin Pharmaceutical CO. , Harbin 150056, China
Abstract:Objective To establish determined method of paeoniflorin in Shugan Pills.Methods C_(18) column was used with methyl alcohol-water(25∶75) as mobil phase and the detecting wavelength at 243 nm.Results The linear range of paeoniflorin was 0.20~1.00 ug,the average recovery rate was 99.88% and RSD was 1.41%,respectively.Conclusion The method was simple and reliable,and could be used for the control quality of paeoniflorin in Shugan Pills.
Keywords:Shugan Pills  paeoniflorin  HPLC
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