| 橘红丸（大蜜丸）及蜂蜜中5-羟甲基糠醛含量测定 |
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| 引用本文： | 谢强胜,谢春红,王坤,李启艳,徐丽华.橘红丸（大蜜丸）及蜂蜜中5-羟甲基糠醛含量测定[J].中国药事,2013,27(6):597-599. |
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| 作者姓名： | 谢强胜 谢春红 王坤 李启艳 徐丽华 |
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| 作者单位： | 1. 山东省食品药品检验所,济南,250101
2. 青岛市黄岛区中医院 |
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| 摘 要： | 目的建立橘红丸（大蜜丸）及蜂蜜中5-羟甲基糠醛的含量测定方法。方法采用Thermo BDSHypersil C18色谱柱,甲醇-0.1%磷酸溶液（4∶96）为流动相,流速为1.0 mL.min-1,检测波长为284nm。结果与结论41批橘红丸（大蜜丸）中,5-羟甲基糠醛含量范围为0.15～32.32mg.g-1。21批蜂蜜中5-羟甲基糠醛含量范围为0～2.17mg.g-1。本法简便、准确,可用于橘红丸（大蜜丸）和蜂蜜的质量控制。
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| 关 键 词： | 橘红丸（大蜜丸） 高效液相色谱法 蜂蜜 5-羟甲基糠醛 |
Content Determination of 5-Hydroxymethyl Furfural (5-HMF) in Honey and Juhong Pills (Big Honeyed Pills) |
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| Xie Qiangsheng
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Xie Chunhong
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Wang Kun
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Li Qiyan
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Xu Lihua.Content Determination of 5-Hydroxymethyl Furfural (5-HMF) in Honey and Juhong Pills (Big Honeyed Pills)[J].Chinese Pharmaceutical Affairs,2013,27(6):597-599. |
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| Authors: | Xie Qiangsheng Xie Chunhong Wang Kun Li Qiyan Xu Lihua |
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| Institution: | (Shandong Institute for Food and Drug Control, Jinan 250101; 1Qingdao Huangdao Hospital of Traditional Chinese Medicine) |
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| Abstract: | Objective To establish a method for determination of 5-hydroxymethyl furfural （5-HMF） in honey and Juhong Pills （Big Honeyed Pills）. Methods The quantitative analysis was performed on a Thermo BDS Hypersil C18 column. The mobile phase was methanol-0.1% phosphoric acid （4 ： 96） with a flow rate of 1.0 mL·min-1. The detection UV wavelength was at 284 nm. Results and Conclusion The 5- HMF quantitative range in the 41 batches of Juhong Pills （Big Honeyed Pills） was 0.15-32.32 mg·g^-1, while in the 21 batches of honey was 0-2.17 mg·g^-1. The method was simple, sensitive, and accurate and could be used for the quality control of honey and Juhong Pills （Big Honeyed Pills）. |
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| Keywords: | Juhong Pills （Big Honeyed Pills） HPLC honey 5-HMF |
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